The effect of heat treatment on evolution of the phase composition and microhardness of orthorhombic alloy Ti – 22Al – 25Nb based upon a Ti2AlNb phase (O-phase) is studied. X-ray diffraction, scanning electron microscopy, and electron back-scatter diffraction are used to study alloy phase composition after different treatments. It is shown that the alloy structure contains β/B2- and O-phases, the proportion of which changes on heat treatment. Microstructure and Vickers microhardness of alloy Ti – 22Al – 25Nb are shown to be interrelated in different states.
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Alloy element content provided in atomic fractions expressed as a percentage.
References
D. He, L. Li, W. Guo, et al., “Improvement in oxidation resistance of Ti2AlNb alloys at high temperatures by laser shock peening,” Corros. Sci., 184, 109364(2021).
K. Goyal and N. Sardana, “Mechanical properties of the Ti2AlNb intermetallic: a review,” Trans. Indian Inst. Met., 74, 1839 – 1853(2021).
D. Avinashand S. P. Leo Kumar, “Investigations on surface-integrity and mechanical properties of biocompatible grade Ti – 6Al – 7Nb alloy,” Mater. Technol. (NYNY), 37(1), 1 – 9 (2021).
K. S. Senkevich, O. Z. Pozhoga, E. A. Kudryavtsev, and V. V. Zasypkin, “The effect of hydrogenation on the fracture of Ti2AlNb-based alloy during ball milling,” J. Alloys Compd., 902, 163794 (2022).
Y. Sun, H. Zhang, Z.-p. Wan, et al., “Establishment of a novel constitutive model considering dynamic recrystallization behaviour of Ti – 22Al – 25Nb alloy during hot deformation,” T. Nonferr. Metal. Soc., 29, 546 – 557 (2019).
L. Shao, S. Wu, A. Datye, et al., “Microstructure and mechanical properties of ultrasonic pulse frequency tungsten inert gas welded Ti – 22Al – 25Nb (at.%) alloy butt joint,” J. Mater. Process. Technol., 259, 416 – 423 (2018).
Y. Longchuan, S. Yan, D. Yulei, and L. Wenhe, “Structural features and mechanical properties of as-cast Ti – 22Al – 25Nb alloy,” Rare Metal Mat. Eng., 49, 42 – 47(2020).
W. Wang, W. Zeng, C. Xue, et al., “Microstructural evolution, creep, and tensile behavior of a Ti – 22Al – 25Nb (at.%) orthorhombic alloy,” Mater. Sci. Eng. A, 603A, 176 – 184(2014).
B. Shao, D. Shan, B. Guo, and Y. Zong, “Plastic deformation mechanism and interaction of B2, α2, and O phases in Ti 22Al 25Nb alloy at room temperature,” Int. J. Plast., 113, 18 – 34 (2019).
W. Wang, W. Zeng, C. Xue, et al., “Quantitative analysis of the effect of heat treatment on microstructural evolution and microhardness of an isothermally forged Ti – 22Al – 25Nb (at.%) orthorhombic alloy,” Intermetallics, 45, 29 – 37 (2014).
Shao, S. Wu, S. Zhao, et al., “Evolution of microstructure and microhardness of the weld simulated heat-affected zone of Ti – 22Al – 25Nb (at.%) alloy with continuous cooling rate,” J. Alloys Compd., 744, 487 – 492 (2018).
J.-R. Chen and W.-T. Tsai, “In situ corrosion monitoring of Ti – 6Al – 4V alloy in H2SO4/HCl mixed solution using electrochemical AFM,” Electrochim. Acta, 56, 1746 – 1751 (2011).
C. Xue, W. Zeng, B. Xu, et al., “B2 grain growth and particle pinning effect of Ti – 22Al – 25Nb orthorhombic intermetallic alloy during heating process,” Intermetallics, 29, 41 – 47 (2012).
S. R. Dey, S. Suwas, J. J. Fundenberger, and R. K. Ray, “Evolution of crystallographic texture and microstructure in the orthorhombic phase of a two-phase alloy Ti – 22Al – 25Nb,” Intermetallics, 17, 622 – 633 (2009).
V. A. Esin, R. Mallick, M. Dadé, et al., “Combined synchrotron x-ray diffraction, dilatometry and electrical resistivity in situ study of phase transformations in a Ti2AlNb alloy,” Mater. Charact., 169, 110654 (2020).
P. Zhang,W. Zeng, R. Jia, et al., “Tensile behavior and deformation mechanism for Ti – 22Al – 25Nb alloy with lamellar O microstructures,” Mater. Sci. Eng. A, 803A, 140492 (2021.)
L. Germann, D. Banerjee, J. Y. Guédou, and J. L. Strudel, “Effect of composition on the mechanical properties of newly developed Ti2AlNb-based titanium aluminide,” Intermetallics, 13, 920 – 924 (2005).
Y. X.Wang, K. F. Zhang, and B. Y. Li, “Microstructure and high temperature tensile properties of Ti22Al25Nb alloy prepared by reactive sintering with element powders,” Mater. Sci. Eng. A, 608, 229 – 233 (2014).
C. J. Boehlert, “Part III. The tensile behavior of Ti – Al – Nb O + Bcc orthorhombic alloys,” Metall. Mater. Trans., A32, 1977 – 1988 (2001).
H. Zhang, N. Yan, H. Liang, and Y. Liu, “Phase transformation and microstructure control of Ti2AlNb-based alloys: a review,” J. Mater. Sci. Technol., 80, 203 – 216 (2021).
Z. Q. Bu, Y. G. Zhang, L. Yang, et al., “Effect of cooling rate on phase transformation in Ti2AlNb alloy,” J. Alloys Compd., 893, 162364 (2022).
D. Li, S. Hu, J. Shen, et al., “Microstructure and mechanical properties of laser-welded joints of Ti – 22Al – 25Nb/TA15 dissimilar titanium alloys,” J. Mater. Eng. Perform., 25, 1880 – 1888 (2016).
H. Zhang, M. Yang, Y. Xu, et al., “Constitutive behavior and hotwork ability of a hot isostatic pressed Ti – 22Al – 25Nb alloy during hot compression,” J. Mater. Eng. Perform., 28, 6816 – 6826(2019).
C. Leyens, “Environmental effects on orthorhombic alloy Ti – 22Al – 25Nb in air between 650 and 1000°C,” Oxid. Met., 54, 475 – 503 (2000).
This work was supported by the Institute of Technology of Aircraft Engine, Beijing Research Institute of Aviation Engineering. This work was financially supported by the Science and Technology Plan Project of Taizhou (No. 21gya23 and No. 2002gy06). The financial support was also from Zhejiang Public Welfare Technology Application Research Project (No. LGC20E010003).
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Translated from Metallovedenie i Termicheskaya Obrabotka Metallov, No. 5, pp. 42 – 46, May, 2023.
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Shao, L., Chen, Y., Datye, A. et al. Effect of Heat Treatment on Two-Phase Ti – 22Al – 25Nb Alloy Phase Composition and Microhardness. Met Sci Heat Treat 65, 304–308 (2023). https://doi.org/10.1007/s11041-023-00930-1
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DOI: https://doi.org/10.1007/s11041-023-00930-1