Skip to main content
Log in

Study of the Hardness and Elastic Modulus of Cementite in the Structure of Granular Pearlite by the Nano-Indentation Method

  • TECHNICAL INFORMATION
  • Published:
Metal Science and Heat Treatment Aims and scope

The method of nano-indentation is used to study the microhardness and modulus of elasticity of cementite in the structure of granular pearlite in the initial condition (after spheroidizing annealing) and after cold plastic deformation with ε = 34% and ε = 65%. It is shown that both characteristics of the cementite vary non-monotonically with an increase in strain. The results are compared with electron microscope data on the evolution of the deformed structure of granular pearlite.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6

Similar content being viewed by others

References

  1. L. I. Tushinskii, A. A. Bataev, and L. B. Tikhomirova, The Structure of Pearlite and the Design Strength of Steel [in Russian], VO “Nauka,” Novosibirsk (1993).

    Google Scholar 

  2. I. L. Yakovleva, L. E. Kar’kina, T. A. Zubkova, and T. I. Tabatchikova, “Effect of cold plastic deformation on the structure of granular pearlite in carbon steels,” Fiz. Met. Metalloved., 112(1), 105 – 112 (2011).

    Google Scholar 

  3. L. E. Kar’kina, T. A. Zubkova, and I. L. Yakovleva, “Study of the dislocation structure of the cementite of granular pearlite after cold plastic deformation,” Ibid., 114(3), 255 – 263 (2013).

    Google Scholar 

  4. B. M. Drapkin, G. M. Kimstach, and T. D. Molodtsova, “On the hardness of cementite,” Metalloved. Term. Obrab. Met., No. 9, 37 – 38 (1996).

  5. B. M. Drapkin, G. M. Kimstach, and T. D. Molodtsova, “Study of the properties of cementite in hypereutectoid white iron,” Fiz. Met. Metalloved., 82(1), 162 – 164 (1996).

    Google Scholar 

  6. R. A. Savrai, A. V. Makarov, V. M. Schastlivtsev, et al., “Elastic modulus of pearlitic steel and its change during cyclic loading,” Deform. Razrush. Mater., No. 7, 15 – 19 (2010).

  7. Yu. I. Golovin, “Nano-indentation and mechanical properties of solids in submicro-volumes, thin surface layers, and films (survey),” Fiz. Tverd. Tela, 50(12), 2113 – 2142 (2008).

    Google Scholar 

  8. Yu. I. Golovin, Nano-Indentation and Its Capabilities [in Russian], Mashinostroenie, Moscow (2009).

    Google Scholar 

  9. S. A. Firstov, V. F. Gorban’, and E. P. Pechkovskii, “Important problems concerning determination of the deformation, elasticity, and strength characteristics of new materials and structural and phase transformations in them by the indentation method,” in: XLVI International Conference “Important Problems of Strength,” Oct. 15 – 17, 2007, Vitebsk, Belarus, Proc. Conf., Part 2 [in Russian], “VGTU” UB, Vitebsk (2007).

  10. A. M. Krivtsov, “Anomalies in the mechanical characteristics of nanosized objects,” Dokl. Akad. Nauk, 381(3), 345 – 347 (2001).

    Google Scholar 

  11. M. N. Hong, W. T. Reynolds Jr., T. Tarui, and K. Hono, “Atom probe and transmission electron microscopy investigations of heavily drawn pearlitic steel wire,” Metall. Trans. A, 30A(3A), 717 – 727 (1999).

    Article  Google Scholar 

  12. H. G. Read, W. T. Reynolds Jr., K. Hono, and T. Tarui, “Apfim and TEM studies of drawn pearlitic wire,” Scr. Metall., 37(8), 1221 – 1230 (1997).

    Article  Google Scholar 

  13. V. M. Schastlivtsev, T. I. Tabatchikova, I. L. Yakovleva, et al., “Evolution of the structure of cementite in carbon steel. II. Data from NHR spectroscopy,” Fiz. Met. Metalloved. 84(5), 150 – 156 (1997).

    Google Scholar 

  14. V. S. Zolotorevskii, Mechanical Properties of Metals [in Russian], Metallurgiya, Moscow (1983).

    Google Scholar 

  15. D. McLean, Mechanical Properties of Metals [Russian translation], Metallurgiya, Moscow (1965).

    Google Scholar 

  16. V. G. Gavrilyuk, The Distribution of Carbon in Steel [in Russian], Naukova Dumka, Kiev (1987).

    Google Scholar 

Download references

This research was conducted in part with financial support in the form of RFFI Grant No. 1-02-00048 and Youth Grant No. 13-2-NP-346 from the Ural Branch of the Russian Academy of Sciences (RFFI — Russian Foundation for Basic Research).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to T. A. Zubkova.

Additional information

Translated from Metallovedenie i Termicheskaya Obrabotka Metallov, No. 6, pp. 49 – 53, June, 2014.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Zubkova, T.A., Yakovleva, I.L., Kar’kina, L.E. et al. Study of the Hardness and Elastic Modulus of Cementite in the Structure of Granular Pearlite by the Nano-Indentation Method. Met Sci Heat Treat 56, 330–335 (2014). https://doi.org/10.1007/s11041-014-9756-3

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11041-014-9756-3

Keywords

Navigation