This is a study of the production of stable disaggregated colloidal solutions of aluminum oxide and titanium dioxide nanoparticles based on dry nanopowders of these materials obtained by laser vaporization and condensation. Ultrasonic processing and high speed centrifuging of suspensions of the dry powders are used to stabilize colloidal solutions with a narrow size distribution of the particles. Prototype national reference materials for the diameter of nanoparticles of colloidal solutions of aluminum oxide and titanium dioxide are developed and certified.
This is a preview of subscription content, log in via an institution to check access.
Similar content being viewed by others
References
Guidance Manual for the Testing of Manufactured Nanomaterials: OECD Sponsorship Programme, www.oecd.org/officialdocuments/public-displaydocumentpdf/?cote=env/jm/mono(2009)20/ rev&doclanguage=en, accessed April 4, 2014.
V. V. Ivanov, et al., "Durable aluminum oxide ceramic made by pulsed magnetic pressing of composite nanopowders," Ross. Nanotekhnol., 1, No. 1–2, 201–208 (2006).
X. Chen and Samuel S. Mao, "Titanium dioxide nanomaterials: synthesis, properties, modifications, and applications," Chem. Rev., 107, No. 7, 2891–2959 (2007).
R. Bienert, F. Emmerling, and A. F. Thunemann, "The size distribution of "gold standard" nanoparticles," Anal. Bioanal. Chem., 395, 1651–1660 (2009).
G. W. Mulholland et al., "Measurement of 100 nm and 60 nm particle standards by differential mobility analysis," J. Res. NIST, 111, 257–312 (2006).
A. A. Efimov et al., "Determination of the effective radius of the tip of the probe of an atomic force microscope using monodispersed silicon oxide nanoparticles," Metrologiya, No. 10, 32–37 (2013); Measur. Techn., 56, No. 12, 1343–1346 (2013).
M. N. Rittner, "Market analysis of nanostructured materials," Am. Ceram. Soc. Bull., 81, 33–36 (2002).
R. A. Andrievskii, "Production and properties of nanocrystalline refractory compounds," Usp. Khimii, 63, No. 5, 431–448 (1994).
A. I. Gusev, Nanomaterials, Nanostructures, and Nanotechnologies, Fizmatlit, Moscow (2009).
Yu. A. Kotov, "Electric explosion of wires as a method for preparation of nanopowders," J. Nanopart. Res., 5, No. 5–6, 539–550 (2003).
Yu. A. Kotov et al., "Study of the characteristics of nanopowders produced by vaporization of a target with a pulsed CO2 laser," Zh. Tekh. Fiz., 72, No. 11, 76–82 (2002).
Yu. A. Kotov and V. V. Ivanov, "Powder nanotechnologies for creation of functional materials and electrochemical power devices," Vest. RAN, 78, 9, 777–791 (2008).
V. R. Khrustov, Development and Study of Ceramics Based on Nanopowders of the Oxides of Aluminum, Zirconium, and Cerium: Auth. Abstr. Dissert. Cand. Techn. Sci., Ekaterinburg (2010).
E. G. Kalinina et al., "Production of suspensions based on aluminum oxide nanopowder with a narrow particle size distribution," Ross. Nanotekhnol., 8, No. 7–8, 78–83 (2013).
MI 2838-2003, GSI. Reference Materials for the Composition and Properties of Substances and Materials. General Specifications for Certification Programs and Methods.
GOST R 8.563-2009, GSI. Measurement Techniques (methods).
RMG 93-2009, GSI. Evaluating the Metrological Characteristics of Reference Materials.
R 50.2.031-2003, GSI. Reference Materials for the Composition and Properties of Substances and Materials. Technique for Evaluating Stability Characteristics.
Author information
Authors and Affiliations
Corresponding author
Additional information
Translated from Izmeritel'naya Tekhnika, No. 8, pp. 5–9, August, 2014.
Rights and permissions
About this article
Cite this article
Lizunova, A.A., Kalinina, E.G., Beketov, I.V. et al. Development of Reference Materials for the Diameter of Nanoparticles of Colloidal Solutions of Aluminum Oxide and Titanium Dioxide. Meas Tech 57, 848–854 (2014). https://doi.org/10.1007/s11018-014-0547-4
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11018-014-0547-4