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Sol–gel synthesis of calcium hydroxyapatite thin films on quartz substrate using dip-coating and spin-coating techniques

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Abstract

Sol–gel synthesis route was suggested to prepare calcium hydroxyapatite (Ca10(PO4)6(OH)2, CHA) thin films on quartz substrates. CHA thin films were obtained using dip-coating and spin-coating techniques by coating the substrates 1, 5, 15 and 30 times. In the sol–gel process, the ethylenediaminetetraacetic acid and 1,2-ethandiol as complexing agents were used. Moreover, triethanolamine and polyvinyl alcohol were used as gel network forming materials. After each coating procedure the films were annealed at 1,000 °C. The results obtained from dip-coating and spin-coating techniques were compared in this study. It was demonstrated, that the formation of calcium hydroxyapatite depends on dipping (or spinning) time and annealing duration.

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Acknowledgments

This research was funded by COST Action MP1202.

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Authors and Affiliations

  1. Department of Inorganic Chemistry, Vilnius University, Naugarduko 24, 03225, Vilnius, Lithuania

    Milda Malakauskaite-Petruleviciene, Zivile Stankeviciute, Aldona Beganskiene & Aivaras Kareiva

  2. Department of Applied Chemistry, Vilnius University, Naugarduko 24, 03225, Vilnius, Lithuania

    Zivile Stankeviciute

Authors
  1. Milda Malakauskaite-Petruleviciene
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  2. Zivile Stankeviciute
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  3. Aldona Beganskiene
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  4. Aivaras Kareiva
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Correspondence to Aivaras Kareiva.

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Malakauskaite-Petruleviciene, M., Stankeviciute, Z., Beganskiene, A. et al. Sol–gel synthesis of calcium hydroxyapatite thin films on quartz substrate using dip-coating and spin-coating techniques. J Sol-Gel Sci Technol 71, 437–446 (2014). https://doi.org/10.1007/s10971-014-3394-5

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  • DOI: https://doi.org/10.1007/s10971-014-3394-5

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