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Impregnation of covalent organic framework into porous silica support for the recovery of palladium ions from simulated high-level liquid waste

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Abstract

In the present study, a porous silica-based covalent organic framework incorporated composite was prepared using a solvothermal reaction and the following wet-impregnation method. Multiple characterization methods including Scanning electron microscope, Fourier transform infrared spectroscopy, X-ray powder diffraction confirmed the surface morphology, thermal stability, and pore structure of the as-prepared composite. The adsorption performances of the prepared composite toward palladium [Pd(II)] from simulated high-level liquid waste were systematically investigated using batch experiments under the effect of contact time, solution temperature, and nitric acid solution.

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Authors and Affiliations

  1. Department of Quantum Science and Energy Engineering, Graduate School of Engineering, Tohoku University, Sendai, Miyagi, 980-8579, Japan

    Hao Wu, Tatsuya Kudo, Tadayuki Takahashi & Seong-Yun Kim

  2. Japan Atomic Energy Agency, Tokai, Ibaraki, Japan

    Tatsuya Ito

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  1. Hao Wu
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  2. Tatsuya Kudo
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  3. Tadayuki Takahashi
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  5. Seong-Yun Kim
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Wu, H., Kudo, T., Takahashi, T. et al. Impregnation of covalent organic framework into porous silica support for the recovery of palladium ions from simulated high-level liquid waste. J Radioanal Nucl Chem 330, 1065–1074 (2021). https://doi.org/10.1007/s10967-021-07971-x

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  • DOI: https://doi.org/10.1007/s10967-021-07971-x

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