Skip to main content
Log in

Experimental studies on hydrogen evolution from zirconium alloy based matrices using TGA-EGA

  • Published:
Journal of Radioanalytical and Nuclear Chemistry Aims and scope Submit manuscript

Abstract

Main techniques used for measurement of Heq in zirconium based alloys (being used as major reactor components for PHWRs) are differential scanning calorimetry, hot vacuum extraction-mass spectrometry and inert gas fusion/extraction technique. In this paper, experimental studies on hydrogen evolution from zirconium based alloys have been reported as a function of temperature using thermogravimetric analysis coupled with evolved gas analysis. The present work is oriented towards studying the extraction characteristics of hydrogen in zirconium based matrices.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Subscribe and save

Springer+ Basic
$34.99 /Month
  • Get 10 units per month
  • Download Article/Chapter or eBook
  • 1 Unit = 1 Article or 1 Chapter
  • Cancel anytime
Subscribe now

Buy Now

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2

Similar content being viewed by others

References

  1. Bajaj SS, Gore AR (2006) Nucl Eng Des 236:701–722

    Article  CAS  Google Scholar 

  2. Hussain A, Al-Othmany D (2013) J Nat Sci Res 3:98–103

    Google Scholar 

  3. Waterside corrosion in nuclear power plants (1998) IAEA TECDOC-996. http://www-pub.iaea.org/MTCD/publications/PDF/te_996_web.pdf. Accessed 26 March 2015

  4. Delayed hydride cracking in zirconium alloys in pressure tube nuclear reactors (2002) IAEA-TECDOC-1410. http://www-pub.iaea.org/MTCD/publications/PDF/te_1410_web.pdf. Accessed 16 April 2015

  5. Singh RN, Kishore R, Sinha TK, Kashyap BP (2002) J Nucl Mater 301:153–164

    Article  CAS  Google Scholar 

  6. Srivastava D, Dey GK, Banerjee S (1995) Metall Trans A 26:270–277

    Article  Google Scholar 

  7. Yadav RB (2007) Hydrogen analysis for QC during pressure tube manufacturing, BRNS theme meeting on assessment of hydrogen damage in PHWR pressure tubes. BARC, Mumbai

    Google Scholar 

  8. Sinha RK, Sinha SK, Madhusoodanan (2008) J Nucl Mater 383:14–21

    Article  CAS  Google Scholar 

  9. Khatamian D, Root B (2008) J Nucl Mater 372:106–113

    Article  CAS  Google Scholar 

  10. Vizcaino P, Banchik AD, Abriata JP (2002) J Nucl Mater 304:96–106

    Article  CAS  Google Scholar 

  11. Bickel GA, Green LW, James MWD, Lamarche TG, Leeson PK, Michel H (2002) J Nucl Mater 306:21–29

    Article  CAS  Google Scholar 

  12. Chandra K, Ramanjaneyulu PS, Yadav CS, Kulkarni AS, Sayi YS, Ramakumar KL (2012) Anal Lett 45:2136–2147

    Article  CAS  Google Scholar 

  13. Standard test method for determination of hydrogen in titanium and titanium alloys by the inert gas fusion thermal conductivity/infrared detection method (2009) ASTM E1447-09. http://compass.astm.org/download/E1447.1604.pdf. Accessed 16 March 2016

  14. Intercomparison of techniques for inspection and diagnostics of heavy water reactor pressure tubes (2009) IAEA-TECDOC-1609. http://www-pub.iaea.org/MTCD/publications/PDF/te_1609_web.pdf. Accessed 16 March 2016

  15. Mallik GK, Alur VD, Akanksha Sinha SK, Yadav CS, Saxena MK, Tomar BS, Anantharaman S (2013) Conference on nuclear and radiochemistry (NUCAR). Jabalpur, India

    Google Scholar 

  16. Llauger JA, Walton GN (1981) J Nucl Mater 97:185–191

    Article  CAS  Google Scholar 

  17. Terrani KA, Balooch M, Wongsawaeng D, Jaiyen S, Olander DR (2010) J Nucl Mater 397:61–68

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Akanksha Samanta.

Electronic supplementary material

Below is the link to the electronic supplementary material.

Supplementary material 1 (DOCX 117 kb)

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Samanta, A., Mallik, G.K. Experimental studies on hydrogen evolution from zirconium alloy based matrices using TGA-EGA. J Radioanal Nucl Chem 310, 469–473 (2016). https://doi.org/10.1007/s10967-016-4800-y

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10967-016-4800-y

Keywords

Navigation