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Quality evaluation of the k 0-standardized neutron activation analysis at the Dalat research reactor

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Abstract

Quality evaluation of the k 0-standardized neutron activation analysis (k 0-NAA) at Dalat research reactor (DRR) has been implemented by analyzing the SMELS, a synthetic multi-element standard material as well as the certified reference materials for purposes of validation and verification of the method. The results revealed that the k 0-NAA established at DRR has met the requirements of multi-element analysis for the intended applications with about 42 elements: Al, As, Au, Ba, Br, Ca, Ce, Cl, Co, Cr, Cs, Cu, Dy, Eu, Fe, Hf, I, In, K, La, Mg, Mn, Mo, Na, Nd, Pr, Rb, Sb, Sc, Se, Sm, Sr, Ta, Tb, Th, Ti, U, V, W, Yb, Zn and Zr in matrices of environment, geology and biology among others. Evaluation criteria for the laboratory quality used in this work are the statistical analysis parameters namely: u-scores, laboratory result/certified value ratios and relative biases as well as the control charts those are shown in the paper.

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Acknowledgments

The financial support through national projects by the MOST of Vietnam is gratefully acknowledged. Our gratitude extends to Mr. Le Vinh Vinh and the DRR’s operators for their kind supporting the implementation of this work. The International Atomic Energy Agency is gratefully acknowledged via TC projects.

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Correspondence to Manh-Dung Ho.

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Ho, MD., Tran, QT., Ho, VD. et al. Quality evaluation of the k 0-standardized neutron activation analysis at the Dalat research reactor. J Radioanal Nucl Chem 309, 135–143 (2016). https://doi.org/10.1007/s10967-016-4795-4

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