Abstract
This paper aims at studying the elementary chemical composition of 70 ceramic fragments from the São Paulo II archaeological site by instrumental neutron activation analysis. The concentration data was studied next using multivariate statistical methods, such as cluster analysis, principal component analysis and discriminant analysis. The results showed three different chemical groups of samples regarding the similarity/dissimilarity between the samples. Ceramics from each group have been selected and dated using thermoluminescence. The firing temperature of the ceramics was determined by electron paramagnetic resonance.
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Munita CS, Barroso LP, Oliveira PMS (2013) Variable selection study using Procrustes analysis. Open J Archaeom 1:31–35
Glascock MD, Speakman RJ, Neff H (2007) Archaeometry at the University of Missouri research reactor and the provenance of obsidian artefacts in North America. Archaeometry 49:343–357
Ocupação Polícroma no Baixo e Médio rio Solimões, Estado do Amazonas. http://www.teses.usp.br/teses/disponiveis/71/71131/tde-05062012-104830/pt-br.php. Accessed 10 October 2014
Arqueologia das campinaranas do baixo rio Negro: em busca dos pré-ceramistas nos areais da Amazônia Central. http://www.teses.usp.br/teses/disponiveis/71/71131/tde-29072009-145147/pt-br.php. Accessed 10 October 2014
Schaan D (2001) Into the labyrinths of Marajoara pottery: status and cultural identity in prehistoric Amazonia. In: McEwan C, Barreto C, Neves EG (eds) Unknown Amazon: culture in nature in ancient Brazil. The British Museum, London
Roosevelt A (1991) Moundbuilders of the Amazon, geophysical archaeology of Marajó Island. Academic Press, San Diego
Evans C, Meggers BJ (1968) Archaeological investigations on the Rio Napo. Smithsonian Institution Press, Washington
Neves EG (2008) Digesta: escritos acerca do direito, do pensamento jurídico, da sua metodologia e outros. In: Silverman H, Isbell W (eds) Handbook of South American Archaeology. Springer, New York
Lima HP, Neves EG, Petersen JB (2006) A fase Açutuba: Um novo complexo cerâmico na Amazônia central. Arqueol Suramericana 2:26–52
Nimuendajú C (1981) Mapa Etnohistórico. Fundação Nacional Pró-Memória - IBGE, Rio de Janeiro
Meggers BJ, Evans C (1957) Archaeological investigations at the mouth of the Amazon. Smithsonian Institution Press, Washington
Meggers BJ (1977) Vegetational fluctuation and prehistoric cultural adaptation in Amazonia: some tentative correlations. World Archaeol 8:287–303
Miller ET (1987) In: Nuñez L, Meggers BJ (eds) Investigaciones paleoindias al sur de la linea ecuatorial. San Pedro de Atacama, Universidad del Norte, Chile
Kern DC, Kämpf N (1989) O efeito de antigos assentamentos indígenas na formação de solos com terra preta arqueológicas na região de Oriximiná - PA. Rev Bras Ciência Solo 13:219–225
Silva FC (2003) Manual de análises químicas de solos, plantas e fertilizantes. EMBRAPA, Brasilia
Falcão NPS, Carvalho EJM, Comerford N (2001) In: Congresso da Sociedade de Arqueologia Brasileira, XI. Grupo de trabalho: Terras Pretas Arqueológicas na Amazônia: Estado da Arte, Rio de Janeiro
Cunha TJF, Madari BE, Benites VM, Canellas LP, Novotny EH, Moutta RO, Trompowsky PM, Santos GA (2007) Fracionamento químico da matéria orgânica e características de ácidos húmicos de solos com horizonte a antrópico da amazônia (Terra Preta). Acta Amazonica 37:91–98
Santos JO, Munita CS, Toyota RG, Vergne C, Silva RS, Oliveira PMS (2009) The archaeometry study of the chemical and mineral composition of pottery from Brazil´s Northeast. J Radioanal Nucl Chem 281:189–192
Cano NF, Machado NG, Gennari RF, Rocca RR, Munita CS, Watanabe S (2012) TL dating of pottery fragments from four archaeological sites in Taquari Valley. Radiat Eff Defects Solids 167:947–953
Cano NF, Ribeiro RB, Munita CS, Watanabe S, Neves EG, Tamanaha EK (2014) Dating and determination of firing temperature of ancient potteries from São Paulo II archaeological site Brazil by TL and EPR techniques. J Cult Herit. doi:10.1016/j.culher.2014.05.010
Cano NF, Turbiani-Filho IT, Munita CS, Souza MC, Angulo R, Watanabe S (2013) TL dating of sediments from Ilha do Mel, Brazil. Quat Int 306:137–145
Zimmerman DW (1971) Thermoluminescent dating using fine grains from pottery. Archaeometry 13:29–52
Watanabe S, Farias TMB, Gennari RF, Ferraz GM, Kunzil R, Chubaci JFD (2008) Chemical process to separate iron oxides particles in pottery sample for EPR dating. Spectrochim Acta A 71:1261–1265
Wintle AG (1997) Luminescence dating: laboratory procedures and protocols. Radiat Meas 27:769–817
Bensimon Y, Deroide B, Clavel S, Zanchetta JV (1998) Electron spin resonance and dilatometric studies of ancient ceramics applied to the determination of firing temperature. Jpn J Appl Phys 37:4367–4372
Bensimon Y, Deroide B, Zanchetta JV (1999) Comparison between the electron paramagnetic resonance spectra obtained in X- and W-bands on a fired clay: a preliminary study. J Phys Chem Solids 60:813–818
Mangueira GM, Toledo R, Teixeira S, Franco RWA (2011) A study of the firing temperature of archeological pottery by X-ray diffraction and electron paramagnetic resonance. J Phys Chem Solids 72:90–96
Bishop RL, Canouts V, Crown PL, Atley SP (1990) Sensitivity, precision, and accuracy: their roles in ceramic compositional data bases. Am Antiq 55:537–546
Glascock MD (1992) Characterization of ceramics at MURR by NAA and multivariate statistics. Prehistory Press, New York
Glascock MD, Neff H (2003) Neutron activation analysis and provenance research in archaeology. Meas Sci Technol 14:1516–1526
Baxter MJ, Freestone C (2006) Log-ratio compositional data analysis in archaeometry. Archaeometry 48:511–531
Hazenfratz R, Mongelo G, Munita CS, Neves EG (2012) Comparison of INAA elemental composition data between Lago Grande and Osvaldo archaeological sites in the central Amazon: a first perspective. J Radioanal Nucl Chem 291:43–48
Oliveira PMS, Munita CS, Hazenfratz R (2010) Comparative study between three methods of outlying detection on experimental results. J Radioanal Nucl Chem 283:433–437
História das caretas: a tradição borda incisa na Amazônia Central. http://www.teses.usp.br/teses/disponiveis/71/71131/tde-22092008-125315/pt-br.php. Accessed 10 October 2014
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This work was supported by the grant from Comissão Nacional de Energia Nuclear—CNEN and CNPq.
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Baria, R., Cano, N.F., Silva-Carrera, B.N. et al. Archaeometric studies of ceramics from the São Paulo II archaeological site. J Radioanal Nucl Chem 306, 721–727 (2015). https://doi.org/10.1007/s10967-015-4183-5
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DOI: https://doi.org/10.1007/s10967-015-4183-5