Skip to main content
Log in

The selective separation of Pu isotopes using molecular recognition technology product AnaLig® Pu02 gel and extraction chromatography TRU® resin

  • Published:
Journal of Radioanalytical and Nuclear Chemistry Aims and scope Submit manuscript

Abstract

Two separation techniques for plutonium determination using IBCS AnaLig® Pu02 molecular recognition technology product (MRT) and extraction chromatography TRU® resin (Eichrom ®Industries) to effectively and selectively separate and recover plutonium were tested. The performance of the methods was successfully tested by analysis of NPL (High Alpha–Beta 2003, 2005) intercomparison sample and radioactive sludge sample from NPP A1 Jaslovské Bohunice with high activities of the plutonium radionuclides. The results obtained for both procedures were compared in terms of activities and recoveries.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6

Similar content being viewed by others

References

  1. Fridlund S, Littlefield S, Rivers I (1994) Commun Soil Sci Plant Anal 25:933

    Article  CAS  Google Scholar 

  2. Matejovic I, Durackova A (1994) Commun Soil Sci Plant Anal 25:1277

    Article  CAS  Google Scholar 

  3. Mitra (ed) (2003) Sample preparation techniques in analytical chemistry. Wiley-Interscience, NJ

    Google Scholar 

  4. Baxter DC, Nichol R, Littlejohn D (1992) Spectrochim Acta 47:1155

    Article  Google Scholar 

  5. Cabrera C, Madrid Y, Camara C (1994) J Anal At Spectrom 9:1423

    Article  CAS  Google Scholar 

  6. Cabrera C, Gallego C, Lopez M, Lorenzo ML (1994) J AOAC Int 77:1249

    CAS  Google Scholar 

  7. Towler PH, Smith JD (1994) Anal Chim Acta 292:209

    Article  CAS  Google Scholar 

  8. IBC Advanced Technologies: AnaLig Gel Data Sheet Plutonium Column Series Pu-02, IBC Advanced Technologies, Inc

  9. Eichrom (1995) Eichrom analytical products description. Eichrom Industries, Inc, MN

    Google Scholar 

  10. Dietz M, Horwitz E(1993) Novel chomatographic materials based in nuclear waste processing chemistry, LC-GC—The Magazine of Separation Science, Vol 11, No. 6

  11. Qiao J et al. (2009) Determination of plutonium isotopes in waters and environmental solids: a review. Anal Chim Acta. doi:10.1016/j.aca.2009.03.010

  12. Kaye JH, Strebin RS, Orr R (1995) J Radioanal Nucl Chem 194:191–196

    Article  CAS  Google Scholar 

  13. Hindman FD (1983) Anal Chim 55:2460

    Article  CAS  Google Scholar 

  14. Sill CW (1987) Nucl Chem Waste Manag 7:201

    Article  CAS  Google Scholar 

Download references

Acknowledgments

This work was supported by the Slovak Research and Development Agency under the contract No. APVV-20-007105.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Silvia Dulanská.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Dulanská, S., Remenec, B., Mátel, Ľ. et al. The selective separation of Pu isotopes using molecular recognition technology product AnaLig® Pu02 gel and extraction chromatography TRU® resin. J Radioanal Nucl Chem 287, 841–845 (2011). https://doi.org/10.1007/s10967-010-0836-6

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10967-010-0836-6

Keywords

Navigation