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Effect of Microwave Heat Treatment on Hydrothermal Synthesis of Nano-MgFe2O4

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Abstract

Microwave sintered magnesium ferrite (MF) nanoparticles are synthesised by hydrothermal technique. X-ray diffraction revealed pure spinel phase but low crystallinity. Synthesised MF is observed to be in nanoscale under scanning electron and transmission electron microscopes. MF is characterised further by Fourier transform infrared and UV-visible spectrometers for vibrational bands and optical band gap information. Electric and magnetic characterizations revealed low conductivity, dielectric loss, magnetic loss and fairly good initial permeability. High coercivity and M-H loop area of MF indicate the hard magnetic nature.

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Acknowledgements

Authors acknowledge SIFat SAS, VIT University, Vellore and Dr. S. Manjunatha Rao from Central University Hyderabad for providing XRD, FTIR and VSM facilities respectively.

Funding

This work is financially supported by DRDO Project: ERIP/EP/1103015/M/01/1484, New Delhi.

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Authors and Affiliations

  1. Ceramic Composite Laboratory, Center for Crystal Growth, VIT, Vellore, 632014, Tamil Nadu, India

    Chandra Babu Naidu K., Prathap S. & Madhuri W.

  2. Department of Physics, GITAM (Deemed to be University), Bangalore, India

    Chandra Babu Naidu K.

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  1. Chandra Babu Naidu K.
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Correspondence to Madhuri W..

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K., C.B.N., S., P. & W., M. Effect of Microwave Heat Treatment on Hydrothermal Synthesis of Nano-MgFe2O4. J Supercond Nov Magn 33, 417–425 (2020). https://doi.org/10.1007/s10948-019-05194-6

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  • DOI: https://doi.org/10.1007/s10948-019-05194-6

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