Abstract
The magnetic behavior of Ni0.05Zn0.95Fe2O4 nanoparticles synthesized by the sol–gel technique route was clarified To figure out the influence of annealing temperature on the structure of Ni0.05Zn0.95Fe2O4 particles, x-ray diffraction (XRD) tool was used and revealed spinel cubic structure without any secondary phases. The particle formation and sizes were obtained using scanning electron microscope (SEM). Elemental composition of the nanoparticles was also provided by an energy-dispersive x-ray analysis tool (EDX). The magnetic behaviors of the synthesized powders annealed at varying temperatures were determined by vibrating sample quantum design PPMS measurement system tool. The M–H curves of the samples showed that the samples had S-shape but they reached no saturation state at the presence even at 30 kOe.
Similar content being viewed by others
References
Gorter, E.W.: Saturation magnetization and crystal chemistry of ferrimagnetic oxides. Philips Res. Repts. 9, 295–320 (1954)
Selim, M.S., Turkey, G., Shouman, M.A., El-Shobaky, G.A.: Solid State Ionics. 120, 173 (1999)
Deraz, N.M., Alarii, A.: Structural, morphological and magnetic properties of nano-crystalline zinc substituted cobalt ferrite system. J. Anal. Appl. Pyrolysis 94, 41–47 (2012)
Ozin, G.A.: Characterization of semiconductor heterostructures and nanostructures. Adv. Mater. 4, 612 (1992)
Gleiter, H.: Nanostructured Materials. Adv. Mater. 4, 474 (1992)
Zhou, Z.H., Xue, J.M., Wang, J., Chan, H.S. O., Yu, T., Shen, Z.X.J.: NiFe2O4 nanoparticles formed in situ in silica matrix by mechanical activation. Appl. Phys. 91, 6015 (2002)
Heiba, Z.K., Mohamed, M.B., Arda, L., Dogan, N.: Cation distribution correlated with magnetic properties of nanocrystalline gadolinium substituted nickel ferrite. J. Magn. Magn. Mater. 391, 195–202 (2015)
Heiba, Z.K., Mohamed, M.B., Wahba, A.M., Arda, L.: Magnetic and structural properties of nanocrystalline cobalt-substituted magnesium–manganese ferrite. J. Supercond. Nov. Magn. 28, 2517–2524 (2015)
Dogan, N., Bingolbali, A., Arda, L., Akcan, D.: Synthesis, structure, and magnetic properties of Ni1−xZn x Fe2O4 Nanoparticles. doi:10.1007/s10948-016-3899-y
Shinde, S.S., Jadhav, K.M.: Electrical and dielectric properties of silicon substituted cobalt ferrites. Mater. Lett. 37, 63–67 (1998)
Sawataky, G.A., Van Der Woude, F., Morrish, A.H.: Cation distributions in octahedral and tetrahedral sites of the ferrimagnetic spinel CoFe2O4. J. Appl. Phys. 39, 1204 (1968)
Rondinone, A.J., Samia, A.C.S., Zhang, Z.J.: Characterizing the magnetic anisotropy constant of spinel cobalt ferrite nanoparticles. Appl. Phys. Lett. 76, 3624–3626 (2000)
Pallai, V., Shah, D.O.: Synthesis of high-coercivity cobalt ferrite particles using water-in-oil microemulsions. J. Magn. Magn. Mater. 163, 243–248 (1996)
Skomski, R.: Nanomagnetics. J. Phys. Condens. Matter. 15, R841–934 (2003)
Ramankutty, C.G., Sugunan, S.: Surface properties and catalytic activity of ferrospinels of nickel, cobalt and copper, prepared by soft chemical methods. Appl. Catal. A 218, 39–51 (2001)
Reddy, C.V.G., Manorama, S.V., Rao, V.J.: Semiconducting gas sensor for chlorine based on inverse spinel nickel ferrite. Sens. Actuators B: Chemical 55, 90–95 (1999)
Candlish, I.E., Kear, B.H., Kim, B.K.: Processing and properties of nanostructured WC-Co. Nanostuct. Mater. 1, 119–124 (1992)
Skandan, G., Hahn, H., Roddy, M., Cannon, W.R.: Ultrafine-grained dense monoclinic and tetragonal zirconia. J. Am. Ceram. Soc. 77, 1706–1710 (1994)
Kishimoto, M., Sakurai, Y., Ajima, T.: Magneto-optical properties of Ba-ferrite particulate media. J. Appl. Phys. 76, 7506–7509 (1994)
Li, F., Liu, J.J., Evans, D.G., Duan, X.: Stoichiometric synthesis of pure MFe2O4 (M = Mg, Co, and Ni) spinel ferrites from tailored layered double hydroxide (hydrotalcite-like) precursors. Chem. Mater. 16, 1597–1602 (2004)
Goya, G.F., Rechenberg, H.R.: Ionic disorder and Néel temperature in ZnFe2O4 nanoparticles. J. Magn. Magn. Mater. 196, 191–192 (1999)
Kasapoglu, N., Birsoz, B., Baykal, A., Koseoglu, Y., Toprak, M.S.: Synthesis and magnetic properties of octahedral ferrite Ni χ Co1– χ Fe2O4 nanocrystals. Cent. Eur. J. Chem. 5, 570–580 (2007)
Baykal, A., Kasapoglu, N., Koseoglu, Y., Toprak, M.S., Bayrakdar, H.: CTAB-assisted hydrothermal synthesis of NiFe2O4 and its magnetic characterization. J. Alloys Compounds 464, 514–518 (2008)
Lutterotti, L.: Maud 2.33, http://www.ing.unitn.it/~maud/
El Sayed, A.M.: Ceram. Int. 28, 363–367 (2002)
Sheikh, A.D., Mathe, V.L.: Anomalous electrical properties of nanocrystalline Ni–Zn ferrite. J. Mater. Sci. 43, 2018 (2008)
Koseoglu, Y., Yildiz, H., Yılgın, R.: Synthesis, characterization and superparamagnetic resonance studies of znfe2 o 4 nanoparticles. J. Nanosci. Nanotechnol. 12, 2261–2269 (2012)
Nathani, H., Misra, R.D.K.: Surface effects on the magnetic behavior of nanocrystalline nickel ferrites and nickel ferrite-polymer nanocomposites. Mater. Sci. Eng. 113, 228 (2004)
Acknowledgments
The support was provided by the Research Fund of Bahcesehir University with the project no: BAU-2010.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Arda, L., Dogan, N. & Boyraz, C. Effects of Annealing Temperature on Microstructure and Magnetic Properties of Ni0.05Zn0.95Fe2O4 Nanoparticles. J Supercond Nov Magn 31, 365–371 (2018). https://doi.org/10.1007/s10948-017-4203-5
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s10948-017-4203-5