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Synthesis and Characterization of Bi1.6Pb0.4Sr2Ca2Cu3O7 Superconducting Oxide by High-Energy Milling

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Abstract

Superconducting Bi1.6Pb0.4Sr2Ca2Cu3O7 was prepared by a solid-state reaction using high-energy milling for the starting materials. The effects of the sintering temperature and time on the phase evolution, microstructure, and superconducting properties were examined by thermogravimetric analysis, X-ray diffraction, scanning electron microscopy, and four-point probe resistivity measurements. High-energy milling decreased the precursor particle size to approximately 30 nm with a relatively uniform distribution of multi-compositions. Because of the mechanochemical activation for the starting materials, the reaction temperature was decreased to 750 ∘C due to the decreased diffusion length required for the solid-state reaction. Bi1.6Pb0.4Sr2Ca2Cu3O7 prepared by high-energy milling showed good superconducting properties with T c∼ 100 K, which is superior to the same material prepared by ball milling and sol-gel routes.

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Acknowledgments

This study was supported by the National Research Foundation of Korea (NRF) grant funded by the Korea government (MSIP) (No. NRF-2014K2A4A1035029). This program was also supported by the Indonesian research fund for competitive research for advanced materials and nanotechnology 2014.

Conflict of interests

The authors have no conflicts of interest to declare.

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Authors and Affiliations

  1. School of Materials Science and Engineering, Yeungnam University, Gyeongsan, 712-749, South Korea

    Nono Darsono, Kati Raju & Dang-Hyok Yoon

  2. Research Center for Metallurgy of Materials, Indonesian Institute of Sciences, Gd. 470, Kawasan Puspiptek, Serpong, Tangerang Selatan, 15314, Indonesia

    Nono Darsono & Agung Imaduddin

Authors
  1. Nono Darsono
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  2. Agung Imaduddin
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  3. Kati Raju
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  4. Dang-Hyok Yoon
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Corresponding author

Correspondence to Dang-Hyok Yoon.

Additional information

Nono Darsono holds a PhD degree at Yeungnam University.

Agung Imaduddin holds a PhD degree at Indonesian Institute of Sciences.

Kati Raju holds a PhD degree at Yeungnam University.

Dang-Hyok Yoon holds a PhD degree at Yeungnam University.

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Darsono, N., Imaduddin, A., Raju, K. et al. Synthesis and Characterization of Bi1.6Pb0.4Sr2Ca2Cu3O7 Superconducting Oxide by High-Energy Milling. J Supercond Nov Magn 28, 2259–2266 (2015). https://doi.org/10.1007/s10948-015-3036-3

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  • DOI: https://doi.org/10.1007/s10948-015-3036-3

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