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Synthesis, Electrical and Magnetic Characterization of Polyacrylamide Hydrogels Including NiFe2O4 Nanoparticles

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Abstract

This study investigates synthesis and characterization of polyacrylamide (PAAm) hydrogels containing magnetic NiFe2O4 nanoparticles. Structural, electrical, and magnetic characterization of the gels have been performed with X-ray powder diffractometry, scanning electron microscopy, DC conductivity, magnetization and fluorescence spectroscopy techniques. Fluorescence and electrical measurements show that nanoparticles have got trapped in the gel so it cannot move through the gel even if the gel is swollen and the voltage is applied. It was observed that the presence of NiFe2O4 nanoparticles makes the gel more homogeneous. Magnetization measurements reveal that NiFe2O4 nanoparticles have superparamagnetic behavior and total magnetization of the gel does not change as the swelling ratio increases. These features make the gel very suitable for applications like magnetic adsorbents.

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References

  1. Satarkar, N.S., Hilt, J.Z.: Acta Biomater. 4, 11 (2008)

    Article  Google Scholar 

  2. Kim, J.Y., Lee, S.B., Kim, S.J., Lee, Y.M.: Polymer 43, 7549 (2002)

    Article  Google Scholar 

  3. Kim, S.Y., Lee, Y.M.: J. Appl. Polym. Sci. 74, 1752 (1999)

    Article  Google Scholar 

  4. Deng, Y., Yang, W., Wang, C., Fu, S.: Adv. Mater. 15, 1729 (2003)

    Article  Google Scholar 

  5. Horak, D., Babic, M., Makova, H., Benes, M.J.: J. Sep. Sci. 30, 1751 (2007)

    Article  Google Scholar 

  6. Inglis, D.W., Riehn, R., Austin, R.H., Sturm, J.C.: Appl. Phys. Lett. 85, 5093 (2004)

    Article  ADS  Google Scholar 

  7. Latham, A.H., Williams, M.E.: Accounts Chem. Res. 41, 411 (2008)

    Article  Google Scholar 

  8. Oh, J.K., Drumright, R., Siegwart, D.J., Matyjaszewski, K.: Prog. Polym. Sci. 33, 448 (2008)

    Article  Google Scholar 

  9. Baghi, M., Mack, M.G., Hambeck, M., Rieger, J., Vogl, T., Gstoettner, W., Knecht, R.: Anticancer Res. 25, 3665 (2005)

    Google Scholar 

  10. Ban, I., Stergar, J., Drofenik, M., Ferk, G., Makovec, D.: J. Magn. Magn. Mater. 323, 2254 (2011)

    Article  ADS  Google Scholar 

  11. Kizildereli, N., Gelir, A., Guney, O., Yilmaz, Y.: J. Appl. Polym. Sci. 115(4), 2455 (2010)

    Article  Google Scholar 

  12. Yılmaz, Y., Uysal, N., Gelir, A., Guney, O., Aktas, D.K., Gogebakan, S., Oner, A.: Spectrochim. Acta. Part A: Mol. And Biomol. Spectrosc. 72(2), 332 (2009)

    Article  ADS  Google Scholar 

  13. Yilmaz, Y., Gelir, A., Alveroglu, E., Uysal, N.: Phys. Rev. E. 77, 051121 (2008)

    Article  ADS  Google Scholar 

  14. Kaya, D., Pekcan, O., Yılmaz, Y.: Phys. Rev. E 69, 016117 (2004)

    Article  ADS  Google Scholar 

  15. Gelir, A., Alveroğlu, E., Tulun, M., Yılmaz, Y., Sözeri, H.: Polym. Eng. Sci. 50(4), 843 (2010)

    Article  Google Scholar 

  16. Kasapoğlu, N., Birsöz, B., Baykal, A., Köseoğlu, Y., Toprak, M.S.: Cent. Eur. J. Chem. 5(2), 570 (2007)

    Article  Google Scholar 

  17. Kasapoğlu, N., Baykal, A., Toprak, M.S., Köseoğlu, Y., Bayrakdar, H.: Turk. J. Chem. 31(6), 659 (2007)

    Google Scholar 

  18. Baykal, A., Kasapoğlu, N., Köseoğlu, Y., Toprak, M.S., Bayrakdar, H.: J. Alloys Compd. 464(1–2), 514–518 (2008)

    Article  Google Scholar 

  19. Baykal, A., Kasapoğlu, N., Durmuş, Z., Kavas, H., Toprak, M.S., Köseoğlu, Y., Turk, J.: Chem. 33, 33–45 (2009)

    Google Scholar 

  20. Kavas, H., Kasapoğlu, N., Baykal, A., Köseoğlu, Y.: Chem. Pap. 63(4), 450 (2009)

    Article  Google Scholar 

  21. Pielaszek, R.: Analytical expression for diffraction line profile for polydispersive powders. In: Appl. Crystallography, Proceedings of the XIX Conference, Kraków, Poland, September, p. 43 (2003)

    Google Scholar 

  22. Wejrzanowski, T., Pielaszek, R., Opalinska, A., Matysiak, H., Łojkowski, W., Kurzydłowski, K.J.: Appl. Surf. Sci. 253, 204 (2006)

    Article  ADS  Google Scholar 

  23. Kim, T., Shima, M.: J. Appl. Phys. 101, 09M516 (2007)

    Article  Google Scholar 

  24. Kodama, R.H., Berkowitz, A.E., McNiff, E.J., Foner, S.: Phys. Rev. Lett. 77, 394 (1996)

    Article  ADS  Google Scholar 

  25. Berkowitz, A.E., Lahut, J.A., Jacobs, I.S., Levinson, L.M., Forester, D.W.: Phys. Rev. Lett. 34, 594 (1975)

    Article  ADS  Google Scholar 

  26. Coey, J.M.D.: Phys. Rev. Lett. 27, 1140 (1971)

    Article  ADS  Google Scholar 

  27. Alveroglu, E., Yilmaz, Y.: Nanoscale Res. Lett. 5, 559 (2010)

    Article  ADS  Google Scholar 

  28. Alveroglu, E., Yilmaz, Y.: Macromol. Chem. Phys. 212(14), 1451 (2011)

    Article  Google Scholar 

  29. Alveroglu, E., Gelir, A., Yilmaz, Y.: Macromolecular Symposia 281, 174 (2009)

    Article  Google Scholar 

  30. Yılmaz, Y., Gelir, A., Salehli, F., Nigmatullin, R.R., Arbuzov, A.A.: J. Chem. Phys. 125, 234705 (2006)

    Article  ADS  Google Scholar 

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Acknowledgements

This work is supported by Fatih University under BAP grant no P50021104-B. H. Sözeri thanks to Mr. C. Berk and Dr. Ö. Duygulu for taking SEM micrographs.

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Authors and Affiliations

  1. TUBITAK-UME, National Metrology Institute, PO Box 54, 41470, Gebze-Kocaeli, Turkey

    H. Sözeri

  2. Department of Physics, Istanbul Technical University, 34469, Maslak-Istanbul, Turkey

    E. Alveroğlu

  3. Department of Chemistry, Fatih University, 34500, B. Cekmece-Istanbul, Turkey

    U. Kurtan, M. Şenel & A. Baykal

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  1. H. Sözeri
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  2. E. Alveroğlu
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  3. U. Kurtan
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  4. M. Şenel
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  5. A. Baykal
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Correspondence to H. Sözeri.

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Sözeri, H., Alveroğlu, E., Kurtan, U. et al. Synthesis, Electrical and Magnetic Characterization of Polyacrylamide Hydrogels Including NiFe2O4 Nanoparticles. J Supercond Nov Magn 26, 213–218 (2013). https://doi.org/10.1007/s10948-012-1714-y

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  • DOI: https://doi.org/10.1007/s10948-012-1714-y

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