Journal of Superconductivity and Novel Magnetism

, Volume 25, Issue 8, pp 2771–2775 | Cite as

Synthesis and Characterization of Ferromagnetic Nickel Nanoparticles

  • T. G. Altınçekiç
  • İ. Boz
  • A. C. Basaran
  • B. Aktaş
  • S. Kazan
Original Paper

Abstract

Nickel nanoparticles on mass production scale have been prepared using a modified polyol process with Ni(CH3COO)2⋅4H2O, NaOH, 1,2 propandiol and hydrazinium hydroxide (N2H4∗H2O). A mixture of face centered cubic (fcc) metallic nickel nanoparticles with 12 nm diameter were obtained. We have experimentally studied the structure of nanoparticle by X-ray and Scanning Electron Microscopy (SEM, EDS). The magnetic properties of the prepared Ni film have been studied by Ferromagnetic Resonance (FMR) technique, Vibrating Sample Magnetometer (VSM) and Vector Network Analyzer (VNA). The effective g-factor and magnetic anisotropy constant were determined as geff=2.25 and Keff=85 Oe, respectively.

Keywords

Ni nanoparticles Ferromagnetic resonance Polyol process 

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. 1.
    Roy, A., Srinivas, V., Ram, S., De Toro, J., Mizutani, U.: Phys. Rev. B 71, 184443 (2005) ADSCrossRefGoogle Scholar
  2. 2.
    Nasongkla, N., Bey, E., Ren, J.M., Ali, H., Khemtong, C., Guthi, J.S., Chin, S.F., Sherry, A.D., Boothman, D.A., Gao, J.M.: Nano Lett. 6, 2427 (2006) ADSCrossRefGoogle Scholar
  3. 3.
    Xu, C.J., Xu, K.M., Gu, H.W., Zheng, R.K., Liu, H., Zhang, X.X., Guo, Z.H., Xu, B.: J. Am. Chem. Soc. 126, 9938 (2004) CrossRefGoogle Scholar
  4. 4.
    Bulte, J.W.M., Douglas, T., Witwer, B., Zhang, S.C., Strable, E., Lewis, B.K., Zywicke, H., Miller, B., Van Gelderen, P., Moskowitz, B.M., Duncan, I.D., Frank, J.A.: Nat. Biotechnol. 19, 1141 (2001) CrossRefGoogle Scholar
  5. 5.
    Lewin, M., Carlesso, N., Tung, C.H., Tang, X.W., Cory, D., Scadden, D.T., Weissleder, R.: Nat. Biotechnol. 18, 410 (2000) CrossRefGoogle Scholar
  6. 6.
    Lee, H., Lee, E., Kim, D.K., Jang, N.K., Jeong, Y.Y., Jon, S.: J. Am. Chem. Soc. 128, 7383 (2006) CrossRefGoogle Scholar
  7. 7.
    Willner, I., Katz, E.: Angew. Chem., Int. Ed. Engl. 42, 4576 (2003) CrossRefGoogle Scholar
  8. 8.
    Mornet, S., Vasseur, S., Grasset, F., Duguet, E.: J. Mater. Chem. 14, 2161 (2004) CrossRefGoogle Scholar
  9. 9.
    Tomita, S., Mitsumata, C.: Phys. Rev. B 71, 180414(R) (2005) ADSCrossRefGoogle Scholar
  10. 10.
    Srajer, G., Lewis, L.H., Bader, S.D., et al.: J. Magn. Magn. Mater. 307, 1 (2006) ADSCrossRefGoogle Scholar
  11. 11.
    Rameev, B.Z., Gupta, A., Miao, G., Xiao, G., Yildiz, F., Tagirov, L.R., Akta, B.: Tech. Phys. Lett. 31(9), 802–805 (2005) Google Scholar
  12. 12.
    Akdogan, N., Rameev, B.Z., Dorosinsky, et al.: J. Phys., Condens. Matter 17, L359 (2005) ADSCrossRefGoogle Scholar
  13. 13.
    Koseoglu, Y., Yildiz, F., Salazar-Alvarez, G., et al.: Phys. Status Solidi (b). Basic Solid State Phys. 242, 1712 (2005) ADSCrossRefGoogle Scholar
  14. 14.
    Rameev, B.Z., Yildiz, F., Aktas, B., et al.: Microelectron. Eng. 69, 330 (2003) CrossRefGoogle Scholar
  15. 15.
    Yildiz, F., Kazan, S., Aktas, B., et al.: J. Magn. Magn. Mater. 305, 24 (2006) ADSCrossRefGoogle Scholar
  16. 16.
    Rameev, B., Yildiz, F., Kazan, S., et al.: Phys. Status Solidi A 203, 1503 (2006) ADSCrossRefGoogle Scholar
  17. 17.
    Yu, K., Kim, Dong J., Hun, S. Chung, Liang, H.: Mater. Lett. 57, 3992 (2003) CrossRefGoogle Scholar
  18. 18.
    Kartopu, G., Yalcin, O., Kazan, S., et al.: J. Magn. Magn. Mater. 321, 1142 (2009) ADSCrossRefGoogle Scholar
  19. 19.
    Kazan, S., Sale, A.G., Gatiiatova, J.I., et al.: Solid State Commun. 150, 219 (2010) ADSCrossRefGoogle Scholar
  20. 20.
    Stepanov, A.L., Khaibullin, R.I., Rameev, B.Z., Reinholdt, A., Kreibig, U.: Tech. Phys. Lett. 30(2), 151–153 (2004) ADSCrossRefGoogle Scholar
  21. 21.
    Hegde, M.S., Larcher, D., Dupont, L., Budoin, B., Tekaia-Elhsissen, K., Tarascon, J.M.: Solid State Ion. 93, 33 (1997) CrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media, LLC 2011

Authors and Affiliations

  • T. G. Altınçekiç
    • 1
  • İ. Boz
    • 1
  • A. C. Basaran
    • 2
  • B. Aktaş
    • 2
  • S. Kazan
    • 2
  1. 1.Department of Chemical Engineering, Faculty of EngineeringIstanbul University AvcılarIstanbulTurkey
  2. 2.Department of PhysicsGebze Institute of TechnologyGebzeTurkey

Personalised recommendations