Abstract
The molecular complexes of 1,3,5-tris-m-chlorophenylisocyanurate and ε-caprolactone were synthesized by the reaction of the latter with 3-chlorophenylisocyanate in the presence of triethylamine. Single crystals were grown, and the molecular and crystal structures of the synthesized complexes were investigated.
This is a preview of subscription content, log in via an institution to check access.
Similar content being viewed by others
References
V. E. Shashova, W. Swently, and R. F. Tietz, J. Am. Chem. Soc., 82, 866–873 (1960).
R. G. Arnold, I. A. Nelson, and I. I. Verbane, Chem. Rev., 47–76 (1957).
M. Ya. Tsarfin, V. V. Zharkov, A. K. Zhitinkina, and G. M. Palyutkin, Plast. Massy, No. 4, 8–11 (1987).
M. Ya. Tsarfin, V. V. Zharkov, and A. K. Zhitinkina, Kinet. Katal., 29, No. 5, 1238–1242 (1988).
E. Malčovsky and J. Střešinka, Petrohemia, 28, No. 4, 91–104 (1988).
Ts. M. Frenkel, A. E. Shvorak, A. V. Pankratov, et al., Izv. Akad. Nauk, Ser. Khim., No. 6, 1662–1668 (1996).
H. R. Kricheldorf, J. Polymer Sci., Polymer Chem. Edition, 17, No. 1, 97–109 (2003).
K. Culbins and K. Hamann, Chem. Ber., B94, 3287–3292 (1961).
R. P. Tiger, L. I. Sarynina, S. G. Entelis, Usp. Khim., XLI, No. 9, 1672–1693 (1972).
A. Altomare, G. Cascarano, and C. Giacovazzo, Acta Crystallogr. A, 47, No. 4, 744 (1991).
L. H. Straver and A. J. Schierbeek, MOLEN. Structure Determination System, Vol. 1, Program Description, Nonius B.V. (1994).
A. L. Spek, Acta Crystallogr. A, 46, No. 1, 34 (1990).
Author information
Authors and Affiliations
Corresponding author
Additional information
Original Russian Text Copyright © 2007 by A. A. Yartseva, L. Sh. Koldrov, S. S. Galibeev, V. P. Arkhireev, N. I. Naumkina, I. A. Litvinov, and A. T. Gubaidullin
__________
Translated from Zhurnal Strukturnoi Khimii, Vol. 48, No. 6, pp. 1203–1209, November–December, 2007.
Rights and permissions
About this article
Cite this article
Yartseva, A.A., Koldrov, L.S., Galibeev, S.S. et al. Crystal structure of the molecular complex of 1,3,5-tris-m-chlorophenylisocyanurate with ε-caprolactone. J Struct Chem 48, 1138–1144 (2007). https://doi.org/10.1007/s10947-007-0182-x
Received:
Revised:
Issue Date:
DOI: https://doi.org/10.1007/s10947-007-0182-x