Abstract
N,N,N′,N′-tetra(2-nitrilethyl) ethane-1,2-diamine and N-(2-nitrilethyl)benzylamine hydrobromide were prepared by the addition reaction of acrylonitrile with corresponding amines, and the two structures were determined by X-ray single crystal diffraction. The two compounds crystallize in monoclinic system, and almost no classical hydrogen bond exists in the two crystal structures.
This is a preview of subscription content, log in via an institution to check access.
Similar content being viewed by others
References
D. T. Mowry, Chem. Rev., 42, No. 2.-P. 189–283 (1948).
K. S. Min and M. P. Suh, J. Am. Chem. Soc., 122, No. 29, 6834–6840 (2000).
Y. Kang, S. S. Lee, K. M. Park, et al., Inorg. Chem., 40, No. 27, 7027–7031 (2001).
G. M. Sheldrick, SHELXS-97, Univ. Göttingen, Germany (1997).
G. M. Sheldrick, SHELXL-97, Univ. Göttingen, Germany (1997).
J. Gao, X. Y. Xu, Q. F., et al., Chin. J. Struct. Chem., 23, No. 4, 413–416 (2004).
F. C. Whitmore, H. S. Mosher, R. R. Adams, et al., J. Am. Chem. Soc., 66, No. 5, 725–731 (1944).
Author information
Authors and Affiliations
Additional information
Original Russian Text Copyright © 2006 by J. Gao, X.-Y. Xu, T.-T. Xu, J. Ni, and Q.-L. Liu
__________
Translated from Zhurnal Strukturnoi Khimii, Vol. 47, No. 2, pp. 388–391, March–April, 2006.
Rights and permissions
About this article
Cite this article
Gao, J., Xu, XY., Xu, TT. et al. Crystal and molecular structure of N,N,N′,N′-tetra(2-nitrilethyl) ethane-1,2-diamine and N-(2-nitrilethyl)benzylamine hydrobromide. J Struct Chem 47, 383–386 (2006). https://doi.org/10.1007/s10947-006-0312-x
Received:
Issue Date:
DOI: https://doi.org/10.1007/s10947-006-0312-x