Abstract
The NiO/rGO composites are synthesized via a hydrothermal method followed by annealing treatment with varying graphene oxide concentrations. The structural and morphological characterizations of synthesized samples are done by XRD, FT-IR, Raman, and FE-SEM. The electrochemical supercapacitor performance of prepared electrodes is characterized by CV, GCD, and EIS studies. The NiO/rGO composite achieved the highest specific capacitance of 727.1 F g−1 at 1 mA cm−2 current density and showed good cyclic stability of about 80.4% over 9000 cycles. In a nonenzymatic glucose sensing study, the sensing properties are analyzed by CV and chronoamperometry. The NiO/rGO composite showed the highest glucose sensitivity of 442.4 μA mM−1 cm−2 with correlation coefficient R2 = 0.9964 and LOD of 7.42 μM.
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Acknowledgements
Dr. G. M. Lohar is thankful to DST-SERB, Government of India, for providing funds under the ECRA scheme File No: ECR/2017/002099.
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OCP: Methodology, Writing—original draft. AVF: Characterizations. VGP: Characterizations. HHP: Characterizations. RVS: Review. VJF: Review. GML: Conceptualization, Writing—review & editing.
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Pore, O.C., Fulari, A.V., Parale, V.G. et al. Facile hydrothermal synthesis of NiO/rGO nanocomposite electrodes for supercapacitor and nonenzymatic glucose biosensing application. J Porous Mater 29, 1991–2001 (2022). https://doi.org/10.1007/s10934-022-01313-2
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DOI: https://doi.org/10.1007/s10934-022-01313-2