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Rapid synthesis of La–Ce–silica mesoporous SBA-15-type material via microwave technique

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Abstract

La–Ce–silica mesoporous SBA-15-type material has been rapidly synthesized using microwave technique and characterized by XRD, FT-IR, DRS, and low temperature N2 adsorption–desorption measurement. The results show the La and Ce were successfully incorporated into the framework of SBA-15 molecular sieve and the synthesized material not only retains the hexagonal order and physical properties of purely siliceous SBA-15 but also possesses high surface area and narrow pore-size distribution. Further, the obtained material La–Ce–SBA-15 was used as catalyst support to load active metal Pt for CO oxidation reaction. The results of experiment indicate that the catalytic activity of Pt/La–Ce–SBA-15 is higher than that of the Pt/SBA-15 and Pt/La/Ce/SBA-15.

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Acknowledgments

The project was supported by the National Natural Science Foundation of China (No. 20576021), the Natural Science Foundation of Fujian Province of China (No. E0710004).

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Authors and Affiliations

  1. College of Chemistry and Materials Science, Fujian Normal University, Fuzhou, Fujian, 350007, China

    Guoqian Chen, Yong Zheng, Xuelin Zheng, Xiaonv Shen & Ying Zheng

  2. National Engineering Research Center of Chemical Fertilizer Catalyst, Fuzhou University, Fuzhou, 350002, China

    Yong Zheng

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  1. Guoqian Chen
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  2. Yong Zheng
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  3. Xuelin Zheng
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  4. Xiaonv Shen
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Correspondence to Ying Zheng.

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Chen, G., Zheng, Y., Zheng, X. et al. Rapid synthesis of La–Ce–silica mesoporous SBA-15-type material via microwave technique. J Porous Mater 16, 361–365 (2009). https://doi.org/10.1007/s10934-008-9208-9

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  • DOI: https://doi.org/10.1007/s10934-008-9208-9

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