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Preparation and Characterization of Cinnamon–Clove Compound Essential Oil Microcapsules/Graphene Oxide/Polyvinyl Alcohol/Polylactic Acid Composite Films for White Beech Mushrooms Packaging

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Abstract

This work developed a novel, environmental, and safe cinnamon–clove compound essential oil microcapsules/graphene oxide/polyvinyl alcohol/polylactic acid (CCCEOM/GO/PVA/PLA) composite films for the fresh-keeping packaging of white beech mushrooms and investigated the effects of essential oils and nano-fillers on prolonging food shelf life. Herein, PVA and PLA were blended to reduce the water solubility and improve the mechanical properties of the composites. The lamellar GO, a nucleating agent, was prepared using the modified Hummer method. Clove and cinnamon essential oils have been blended to obtain composite essential oils with better antibacterial activity and encapsulated in beta-cyclodextrin (β-CD) to produce CCCEOM, a sustained-release antibacterial agent. The CCCEOM/GO/PVA/PLA composites were fabricated by integrating GO and CCCEOM into the PVA/PLA matrix, and the morphology, water solubility, optical properties, mechanical properties, thermal stability, and oxygen permeability of the composites were characterized. It was found that the composites demonstrated significant antibacterial activity against Mucor and Aspergillus niger, low water solubility (0.009%), high light transmittance (84.63%), as well as excellent tensile strength (42.29 MPa), and oxygen transmission rate (82.65 cm3/(m2·24 h·0.1 MPa)) with the addition of 0.20 wt% GO and 10 wt% CCCEOM. Moreover, the results of the preservation experiment demonstrate that it can also maintain the quality of white beech mushrooms to some extent and prolong their shelf life for 4 days at 4 °C, which also provides support for their application in food packaging.

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Funding

This work was financially supported by the Fundamental Research Funds for the Central Universities (2572017DB03).

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  1. College of Home and Art Design, Northeast Forestry University, Harbin, 150040, Heilongjiang, People’s Republic of China

    Haoran Zhang, Weijing Sun & Shuyan Xu

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Contributions

Haoran Zhang: Conceptualization, Methodology, Investigation, Software, Formal analysis, Writing—original draft, Writing—review &editing. Weijing Sun: Conceptualization, Methodology, Investigation, Validation. Shuyan Xu: Resources, Supervision, Funding acquisition, Conceptualization, Data curation, Writing—review & editing.

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Correspondence to Shuyan Xu.

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Zhang, H., Sun, W. & Xu, S. Preparation and Characterization of Cinnamon–Clove Compound Essential Oil Microcapsules/Graphene Oxide/Polyvinyl Alcohol/Polylactic Acid Composite Films for White Beech Mushrooms Packaging. J Polym Environ (2024). https://doi.org/10.1007/s10924-024-03188-7

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