Ambient temperature was recorded during experiment and varied between 0.60 and 2.40 °C. The measured temperature on the casing pipe was unchanged, 6.60 °C, before and after the cooling phase. This means the temperature decrease of the service pipe during the cooling procedure has not reached the casing pipe. Furthermore, the thermal inertia of the soil material can be neglected in Eqs. (1–4).
The temperature of the service pipe in the network (A–D) during the cooling phase (175 min) is shown in Fig. 5. The measured temperature decrease was 1.55 °C (from 90.85 to 89.30 °C).
The electrical resistance of the copper wire was measured to 13.466 (Ohm) before start of the cooling phase, which decreased to 13.446 (Ohm) at the end of the cooling phase, see Fig. 6. The temperature at the position of copper wire was calculated by Eq. (5) to a decrease from 71.26 to 70.85 °C. Unlike the service pipe which is in direct contact with the water, the cooling of the copper wire did not start immediately when the valve was switched off.
Calculating Thermal Conductivity by Using Temperature Decrease at the End Part of the Service Pipe
Thermal conductivity in insulation between service pipe and copper wire was calculated to 0.069 W/(m K) at 81 °C by using Eqs. (1–4) and approximating quasi steady state condition for T1 as copper wire temperature. The temperature 81 °C represents the mean temperature between service pipe and copper wire. The calculated thermal conductivity was far from the expected value at this temperature range. The reason was that the measured service pipe temperature at the excavation was not representative for the network (A–D), as mentioned before.
Comparing Calculated and Measured Temperature of the Copper Wire
The position of the copper wire was expected to be at 16.5 mm, the mean value of 15–18 mm, from service pipe. The temperature of the copper wire was calculated at steady state condition, before starting the cooling experiment, by using the measured temperatures of the casing pipe (6.6 °C) and the service pipe (90.85 °C) as the boundary condition. The calculated temperature was 73.50 °C at the copper wire position, approximately 2.2 °C higher than measured (71.26 °C). Assuming the maximum possible distance of the copper wire from the steel service pipe (18 mm), the copper wire temperature was calculated to 71, 80 °C, see Fig. 7.
Determination of Thermal Conductivity by Using Temperature Decrease in the Valve
The absolute temperature for the valve in point B decreased from 85.60 to 84.90 °C, a temperature difference of 0.70 °C, see Fig. 8. The thermal diffusivity of steel offsets the cooling phase for the valve by approximately 60 min.
Removal of the soil in the point A leads to higher heat losses at the measuring point than at the parts which were covered by soil. Hence, the measured service pipe temperature was lower than the actual temperature of the service pipe at the network (A–D). Thus, it was assumed that the temperature decrease of the valve in point B represents the cooling of the service pipe more accurately. Therefore, the measured temperature of the service pipe of the network (A–D) after cooling was adjusted according to Eqs. (6–8).
$$ \frac{{T_{S1} - T_{V1} }}{{T_{V1} }} = P $$
(6)
$$ \left( {P + 1} \right){*}T_{V2} = T_{S2} $$
(7)
$$ \Delta T = T_{S1} - T_{S2} $$
(8)
where \(T_{S1} \;\left( {\text{K}} \right)\) is service pipe temperature before cooling,\( T_{V1} \;\left( {\text{K}} \right)\) is valve temperature before cooling, \(P \left( \% \right)\) is percentual difference between \(T_{S1}\) and \(T_{V1}\), \(T_{V2} \; \left( {\text{K}} \right)\) is valve temperature after cooling, \(T_{S2} \;\left( {\text{K}} \right)\) is service pipe temperature after cooling and \(\Delta T \;\left( {\text{K}} \right)\) is adjusted temperature decrease of service pipe.
The adjusted temperature decrease of the service pipe in the network (A–D) was 0.74 °C. The thermal conductivity of the PUR between the service pipe and the copper wire was calculated to 0.031 W/(m K) at 81 °C by using the adjusted temperature decrease. Furthermore, thermal conductivity of the PUR at 50 °C was calculated to 0.027 W/(m K) by using Eq. (9) [13].
$$ \lambda_{T} = \lambda_{50} + 0.00016{ }(T - 50) $$
(9)
where λT [(W/(m K)] is thermal conductivity, \(\lambda_{50}\) is the thermal conductivity at 50 °C and T (K) is temperature.
Simplified Sensitivity Analysis
According to the producer of the pipes (PowerPipe systems AB), thermal conductivity at 50 °C of a newly produced pipe should not exceed 0.026 W/(m K) [4]. The cooling method was performed on newly installed pipes. The thermal conductivity calculated at 50 °C by the cooling method, 0.027 W/(m K), is in very good agreement with the declare value of the producer. However, accuracy of the calculated thermal conductivity depends strongly on the position of the copper wire. A sensitivity analysis was conducted where the service pipe temperature prior to cooling (90.85 °C), the measured casing pipe temperature (6.60 °C) and the adjusted temperature decrease in the service pipe (0.74 °C) were used to calculate the overall thermal conductivity of the network (A–D), which was calculated to λ50 0.024 W/(m K). The calculated overall thermal conductivity is 9.4% lower compared to the result obtained by using the measurement temperature of the copper wire at 16.5 mm from service pipe.
The thermal conductivity of PUR at 50 °C was calculated to 0.028 W/(m K) by using the measured temperature of the copper wire (71.26 °C) and assuming the 18 mm distance between the copper wire and the service pipe. This results in a difference of 7% compared to the calculated thermal conductivity with the assumption that the copper wire distance was 16.5 mm from service pipe.
A compilation of all calculated thermal conductivities is presented in Table 1.
Table 1 Compilation of calculated thermal conductivities for PUR, at mean temperature for evaluated part of insulation. Together with its corresponding thermal conductivity calculated at 50 °C by Eq. (9) The energy loss during the cooling process corresponded to the temperature decrease (ΔT) in the service pipe, which governs the result. The calculated thermal conductivity at 50 °C 0.027 W/(m K) was related to a temperature decrease of 0.7 °C at the valve in point B and adjusted to 0.74 °C by Eqs. (6–8). A temperature decrease of 0.6–0.8 °C would have resulted in a thermal conductivity of 0.020–0.029 W/(m K).