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Structural, Thermal, Optical and Antibacterial Properties of Co-doped (Dy3+/Eu3+): PEG + PVA Novel Transparent Hybrid Films

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Abstract

In this report, PEG + PVA + Dy3+:Eu3+ films with Eu3+ concentrations of 1–7wt% were prepared by solution casting method and characterized. The composites were characterized by PXRD, FTIR, UV–Vis, DMA, SEM, TGA and photoluminescence measurements, and also their antibacterial activities were tested by the diffusion method. Thermogravimetric analyzes show that increasing Eu3+ content outstandingly increases thermal stability. Moreover, the antibacterial properties of composites showed strong activities against E. coli and S. aureus with the addition of Dy3+ and Eu3+ ions to polymer blends. Optical measurement records presented that the optical band gap Eg progressively decreased from 4.66 eV for the undoped PEG + PVA blend film to 3.18 eV by increasing Eu3+ ions concentration. Charmingly, the room temperature PL results reveal that the enhancement of the emission of Eu3+ ions in the PEG + PVA polymer matrix after co-doping with Eu3+ ions, whereas the reduction of Dy3+ emission intensity, owing to energy migration from Dy3+ to Eu3+. Besides, according with low-temperature PL measurements indicate that the PL density gradually decreases due to thermal quenching as the temperature increases. With the temperature increased, the color coordinates gradually changed from orange to reddish-orange. These results show that Dy3+/Eu3+ doped polymer blends can likely of a promising candidate in varieties of applications including OLEDs, biosensors, polymer solar cells and optoelectronics devices.

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Acknowledgements

The authors are grateful to the Research Funds of Balikesir University (BAP-2019/079) for the financial support and to Balikesir University, Science and Technology Application and Research Center (BUBTAM) for the use of the Photoluminescence Spectrometer, Dynamic Mechanic Analyzer (DMA) and Scanning Electron Microscope (SEM).

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Authors and Affiliations

  1. Center of Sci. and Tech. App. and Research, Balikesir University, Balikesir, Turkey

    Mustafa Burak Coban & Mehmet Emin Diken

  2. Faculty of Science and Literature, Department of Molecular Biology and Genetic, Balikesir University, Balikesir, Turkey

    Serap Dogan

  3. Department of Energy, Graduate School of Natural and Applied Sciences, Mugla Sitki Kocman University, Mugla, Turkey

    Hulya Kara Subasat

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MBC: Conceptualization, methodology, writing—original draft, supervision, software, writing—original draft, writing—review and editing. MED: Conceptualization, visualization and methodology. SD: Software and visualization. HKS: Visualization and methodology. All authors reviewed the manuscript.

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Correspondence to Mustafa Burak Coban.

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Coban, M.B., Diken, M.E., Dogan, S. et al. Structural, Thermal, Optical and Antibacterial Properties of Co-doped (Dy3+/Eu3+): PEG + PVA Novel Transparent Hybrid Films. J Inorg Organomet Polym 33, 2924–2942 (2023). https://doi.org/10.1007/s10904-023-02724-7

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