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Solvent-Mediated 1,ω-Bis(isoquinoline)alkane/Iodobismuthate Hybridized Isomers: Structures and Packing Mode Dependent-Photoluminescence/Thermochromisms

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Abstract

The hybridization of 1,4-bis(isoquinoline)butane (BIQBT2+) cation with iodobismuthate under different solvents produce two isomers α-[(BIQBT)(BiI4)2]n (α-1, in CH3OH/H2O mixed solvent, Triclinic system with P-1 space group) and β-[(BIQBT)(BiI4)2]n (β-1, in CH3OH, Monoclinic system with P21/c space group). The 1-D (BiI4) n−n chains are constructed from the opposite edge-sharing BiI6 octahedra. The (BIQBT)2+ in α-isomer adopts the planar configuration, and that in β-isomer presents the chair-like configuration, as a result, different packing modes (intercalating quasi-3-D mode for α-1 and interlocking 2-D mode for β-1) are observed. Interestingly, from α-1 to β-1, distortion degree of BiI6 octahedron and π–π stacking interaction decrease, but hydrogen bonds number increase. Consequently, due to different packing mode, photoluminescence/thermochromisms can be found in α-1, but those of β-1 are vanished, Theoretical calculation was conducted to disclose the structure/thermochromism correlation.

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Funding

This work was financially supported by National Natural Science Foundation of China (No: 21771038), the Key Fund for the Higher Education Quality Engineering of Anhui Province (Grant No. 2018jyxm0213) and National Natural Science Foundation of Fujian Province (2018J01684).

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Authors and Affiliations

  1. Department of Pharmacy, West Anhui Health Vocational College, Lu’an, 237005, Anhui, China

    Peng Wang & Wen-Wen Sheng

  2. College of Chemistry, Fuzhou University, Fuzhou, 350116, Fujian, China

    Zhi-Rong Chen & Hao-Hong Li

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10876_2020_1829_MOESM1_ESM.pdf

Supplementary material 1 (PDF 313 kb) Crystallographic data for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Center as supplementary publication No.CCDC-1999920, 1010456. Copy of the data can be obtained free of charge at http://www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Center(CCDC), 12 Union Road, Cambridge CB2 1EZ, UK; Fax: +44(0)1223-336033; email:deposit@ccdc.cam.ac.uk)

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Wang, P., Sheng, WW., Chen, ZR. et al. Solvent-Mediated 1,ω-Bis(isoquinoline)alkane/Iodobismuthate Hybridized Isomers: Structures and Packing Mode Dependent-Photoluminescence/Thermochromisms. J Clust Sci 32, 727–735 (2021). https://doi.org/10.1007/s10876-020-01829-0

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