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Synthesis, Structure and Characterisation of One Two-Dimensional Layered Vanadium Tellurite [H2en] n [V2Te2O10] n

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Abstract

A two-dimensional layered organic templated vanadium tellurite, [H2en] n [V2Te2O10] n 1 (en = ethanediamine) has been synthesized through a conventional hydrothermal reaction and structurally characterized by X-ray powder diffraction, X-ray single-crystal diffraction analysis, FTIR, UV-DRS, thermogravimetric analysis (TGA), thermal-dependent 2D-IR correlation spectroscopy (2D-COS IR) and element analysis. Compound 1 is allomorphic to [H2en][V2Te2O5]2 which is reported by Jung et al. According to the data of compound 2 got from the Cambridge Crystallographic Data Centre (CCDC) and Mercury, we optimize the H-bondings of compound 2. The two compounds are compared in weak interactions, IR and TGA characterizations, and UV and thermal-dependent 2D-IR spectroscopy of compound 1 was supplementary reported. Furthermore, we calculated the topology type of both two compounds.

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Acknowledgments

This research was financially supported by the National Science Foundation of China (Grants 21003020), Fujian Provincial Natural Science Foundation (2013J01042), Open Fund of State Key Laboratory of Structural Chemistry (20130015).

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Authors and Affiliations

  1. Department of Chemistry, Fuzhou University, Fuzhou, 350108, People’s Republic of China

    Zhen Yang, Yiping Chen, Zhenqiang Guo, Zhuchai You, YanQiong Sun & Liuqin Su

  2. State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, 350002, Fujian, People’s Republic of China

    Yiping Chen

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  1. Zhen Yang
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Correspondence to Yiping Chen.

Appendix: Supplementary Material

Appendix: Supplementary Material

Crystallographic data for the compound 1 has been deposited with the Cambridge Crystallographic Data Centre (CCDC) as Supplementary Publications CCDC reference number 970648. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB 21 EZ, UK (Fax: +44-1223-336033; e-mail: deposit@ccdc.cam.ac.uk).

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Yang, Z., Chen, Y., Guo, Z. et al. Synthesis, Structure and Characterisation of One Two-Dimensional Layered Vanadium Tellurite [H2en] n [V2Te2O10] n . J Clust Sci 25, 1363–1375 (2014). https://doi.org/10.1007/s10876-014-0714-4

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