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Journal of Cluster Science

, Volume 24, Issue 1, pp 189–195 | Cite as

Preparation and Characterization of NiO Nanoparticles via Solid-State Thermal Decomposition of Ni(II) Complex

  • Aliakbar Dehno KhalajiEmail author
Original Paper

Abstract

Nickel(II) complex, Ni(Brsalph)(NO3) was synthesized and characterized by elemental analyses and Fourier-transformed infrared (FT-IR) spectroscopy. Heating of Ni(Brsalph)(NO3) at 550 °C for 3.5 h have resulted NiO nanoparticles. Fourier-transformed infrared spectrum confirmed the composition of products. The crystalline structures and morphology of NiO nanoparticles were studied by X-ray powder diffraction, scanning electron microscopy and transmission electron microscopy.

Keywords

Nanoparticles NiO Schiff base XRD SEM TEM 

Notes

Acknowledgments

I am grateful to the Council of Iran National Science Foundation and Golestan University for financial support of this work.

References

  1. 1.
    M. Salavati-Niasari, F. Davar, and A. Khansari (2011). J. Alloys Compd. 509, 61–65.CrossRefGoogle Scholar
  2. 2.
    M. Salavati-Niasari, F. Davar, and Z. Fereshteh (2009). Chem. Eng. J. 146, 498–502.CrossRefGoogle Scholar
  3. 3.
    M. Salavati-Niasari, N. Mir, and F. Davar (2008). J. Alloys Compd. 476, 908–912.CrossRefGoogle Scholar
  4. 4.
    Z. RashidiRanjbar and A. Morsali (2011). J. Inorg. Organomet. Polym. 21, 421–430.CrossRefGoogle Scholar
  5. 5.
    M. Khanpour, A. Morsali, and P. Retailleau (2010). Polyhedron 29, 1520–1524.CrossRefGoogle Scholar
  6. 6.
    J. Xu, L. Gao, J. Cao, W. Wang, and Z. Chen (2010). Elctrochim. Acta 56, 732–736.CrossRefGoogle Scholar
  7. 7.
    I. Luisetto, F. Pepep, and E. Bemporad (2008). J. Nanopart. Res. 10, 59–67.CrossRefGoogle Scholar
  8. 8.
    S. Farhadi and K. Pourzare (2012). Mat. Res. Bull. 47, 1550–1556.CrossRefGoogle Scholar
  9. 9.
    G. Sharma and P. Jeevanandam (2012). Appl. Surf. Sci. 258, 3679–3688.CrossRefGoogle Scholar
  10. 10.
    M. Salavati-Niasari, F. Davar, and M. Mazaheri (2008). Polyhedron 27, 3467–3471.CrossRefGoogle Scholar
  11. 11.
    F. Davar, M. Salavati-Niasari, N. Mir, K. Saberyan, M. Monemzadeh, and E. Ahmadi (2010). Polyhedron 29, 1747–1753.CrossRefGoogle Scholar
  12. 12.
    M. Salavati-Niasari and F. Davar (2009). Mat. Lett. 63, 441–443.CrossRefGoogle Scholar
  13. 13.
    Y. R. Uhm, J. H. Park, W. W. Kim, M. K. Lee, and C. K. Rhee (2007). Mat. Sci. Eng. A449, 817–820.Google Scholar
  14. 14.
    X. Jiang, T. Herricks, and Y. Xia (2002). Nano Lett. 2, 1333–1338.CrossRefGoogle Scholar
  15. 15.
    W. Jia, E. Reitz, P. Shimpi, E. G. Rodriguez, P.-X. Gao, and Y. Lei (2009). Mat. Res. Bull. 44, 1681–1686.CrossRefGoogle Scholar
  16. 16.
    A. El-Trass, H. Elshamy, I. El-Mehasseb, and M. El-Kemary (2012). Appl. Surf. Sci. 258, 2997–3001.CrossRefGoogle Scholar
  17. 17.
    H. Sadeghzadeh and A. Morsali (2010). J. Inorg. Organomet. Polym. 20, 733–738.CrossRefGoogle Scholar
  18. 18.
    L. Hashemi and A. Morsali (2010). J. Inorg. Organomet. Polym. 20, 856–861.CrossRefGoogle Scholar
  19. 19.
    H. Sadeghzadeh, A. Morsali, and P. Retailleau (2010). Polyhedron 29, 925–933.CrossRefGoogle Scholar
  20. 20.
    L. Aboutorabi and A. morsali (2010). Inorg. Chim. Acta 363, 2506–2511.CrossRefGoogle Scholar
  21. 21.
    J. Bahadur, D. Sen, S. Mazumder, and S. Ramanathan (2008). J. Sol. State Chem. 181, 1227–1233.CrossRefGoogle Scholar
  22. 22.
    Granqvist (ed.) Handbook of Inorganic Electrochromic Materials (Elsevier, Amsterdam, 1995).Google Scholar
  23. 23.
    I. Hotovy, J. huran, L. Spiess, S. Hascik, and V. Rehacek (1999). Sens. Actuators B57, 147–153.Google Scholar
  24. 24.
    D. Wang, R. Xu, X. Wang, and Y. Li (2006). Nanotechnology 17, 979–983.CrossRefGoogle Scholar
  25. 25.
    S. H. Lin, F. R. Chen, and J. J. Kai (2008). Appl. Surf. Sci. 254, 3357–3363.CrossRefGoogle Scholar
  26. 26.
    Y. R. Uhma, J. H. Park, W. W. Kima, C. H. Chob, and C. K. Rhee (2004). Mater. Sci. Eng. B106, 224–227.CrossRefGoogle Scholar
  27. 27.
    H. Yang, Q. Tao, X. zhang, A. Tang, and J. Ouyang (2008). J. Alloys Compd. 459, 98–103.CrossRefGoogle Scholar
  28. 28.
    P. Poizot, S. Laruelle, S. Grugeon, L. Dupont, and J.-M. Tarascon (2000). Nature 407, 496–499.CrossRefGoogle Scholar
  29. 29.
    D. Y. Han, H. Y. Yang, C. B. Shen, X. Zhou, and F. H. Wang (2004). Powder Technol. 147, 113–116.CrossRefGoogle Scholar
  30. 30.
    C. K. Xu, K. Q. Hong, S. Liu, G. H. Wang, and X. N. Zhao (2003). J. Cryst. Growth 255, 308–312.CrossRefGoogle Scholar
  31. 31.
    Y. J. Zhan, C. R. Yin, C. L. Zheng, W. Z. Wang, and G. H. Wang (2004). J. Solid State Chem. 177, 2281–2284.CrossRefGoogle Scholar
  32. 32.
    W. Z. Wang, Y. K. Liu, C. K. Xu, C. L. Zheng, and G. H. Wang (2002). Chem. Phys. Lett. 362, 119–122.CrossRefGoogle Scholar
  33. 33.
    H. A. Pang, Q. Y. Lu, Y. Z. Zhang, Y. C. Li, and F. Gao (2010). Nanoscale 2, 920–922.CrossRefGoogle Scholar
  34. 34.
    S. A. Needham, G. X. Wang, and H. K. Liu (2006). J. Power Sources 159, 254–257.CrossRefGoogle Scholar
  35. 35.
    M. Salavati-Niasari, N. Mir, and F. Davar (2010). J. Alloys Compd. 493, 163–168.CrossRefGoogle Scholar
  36. 36.
    M. Salavati-Niasari, F. Mohandes, F. Davar, M. Mazaheri, M. Monemzadeh, and N. Yavarinia (2009). Inorg. Chim. Acta 362, 3691–3697.CrossRefGoogle Scholar
  37. 37.
    F. Davar, Z. Fereshteh, and M. Salavati-Niasari (2009). J. Alloys Compd. 476, 797–801.CrossRefGoogle Scholar
  38. 38.
    Z. Fereshteh, M. Salavati-Niasari, K. Saberyan, S. M. Hosseinpour-Mashkani, and F. Tavakoli (2012). J. Clust. Sci. 23, 577–583.CrossRefGoogle Scholar
  39. 39.
    S. Farhadi and Z. Roostaei-Zaniyani (2011). Polyhedron 30, 1244–1249.CrossRefGoogle Scholar
  40. 40.
    M. Salavati-Niasari, N. Mir, and F. Davar (2009). Polyhedron 28, 1111–1114.CrossRefGoogle Scholar
  41. 41.
    S. Farhadi and Z. Roostaei-Zaniyani (2011). Polyhedron 30, 971–975.CrossRefGoogle Scholar
  42. 42.
    B. S. Kwak, B.-H. Choi, M.-J. Ji, S.-M. Park, and M. Kang (2012). J. Ind. Eng. Chem. 18, 11–15.CrossRefGoogle Scholar
  43. 43.
    S. Farhadi, M. Kazem, and F. Siadat Nasab (2011). Polyhedron 30, 606–613.CrossRefGoogle Scholar
  44. 44.
    L. Wang, Y. Hao, Y. Zhao, Q. Lai, and X. Xu (2010). J. Solid State Chem. 183, 2576–2581.CrossRefGoogle Scholar
  45. 45.
    L. A. Saghatforoush, R. Mehdizadeh, and F. Chalabian (2010). Trans. Met. Chem. 35, 903–910.CrossRefGoogle Scholar
  46. 46.
    M. Salavati-Niasari, F. Davar, and Z. Fereshteh (2010). J. Alloys Compd. 494, 410–414.CrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media New York 2012

Authors and Affiliations

  1. 1.Department of Chemistry, Faculty of ScienceGolestan UniversityGorganIran

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