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Journal of Cluster Science

, Volume 24, Issue 1, pp 289–297 | Cite as

Synthesis and Characterization of Nickel Oxide Nanoparticles from Ni(salen) as Precursor

  • Afsaneh Khansari
  • Morteza Enhessari
  • Masoud Salavati-NiasariEmail author
Original Paper

Abstract

Nickel oxide nanoparticles have been synthesized by thermal treatment of N,N′-(bis(salicylidene)-ethylene-1,2-diamine)Nickel(II); [Ni(salen)]; as precursor which has been synthesized via two methods: [Ni(salen)] were obtained by solid state reaction in absence solvent and co-precipitation reaction in presence of propanol as solvent, respectively. Nickel oxide nanoparticles were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and Fourier transform infrared spectroscopy.

Keywords

Nickel oxide Thermal treatment Nanoparticles Solid state reaction 

Notes

Acknowledgments

The authors are grateful to the council of Iran National Science Foundation and University of Kashan for supporting this work by Grant No. (159271/16).

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Copyright information

© Springer Science+Business Media New York 2013

Authors and Affiliations

  • Afsaneh Khansari
    • 1
  • Morteza Enhessari
    • 2
  • Masoud Salavati-Niasari
    • 3
    Email author
  1. 1.Department of Inorganic Chemistry, Faculty of ChemistryUniversity of GuilanRashtIslamic Republic of Iran
  2. 2.Islamic Azad UniversityNaraghIslamic Republic of Iran
  3. 3.Institute of Nano Science and Nano TechnologyUniversity of KashanKashanIslamic Republic of Iran

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