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A New Microporous Hydrogen-Bonding Framework Constructed from 1-(4-Hydroxyphenyl)-5-Thioacetatetetrazole

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Abstract

The new complex with flexible heterocyclic carboxylate ligand, [Ba(HL−)2(H2O)3]·H2O (H2L = 1-(4-Hydroxyphenyl)-5-thioacetatetetrazole), were synthesized and structurally determined by X-ray diffraction analysis. The complex belongs to the monoclinic system, space group C2/c. The center Ba(II) is nine-coordinated by six carboxylate oxygen atoms from four HL-ligands and three water molecules in a distorted monocapped square trans-prism geometry. The ligand serves as a bridge to link two adjacent Ba(II) atoms into a chain structure which are further assembled into the final three-dimensional supramolecular architecture with microporous open channel via hydrogen bonds.

Graphical Abstract

A new complex is assembled into three-dimensional supramolecular architecture with microporous open channel via hydrogen bonds.

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Authors and Affiliations

  1. Zhejiang Key Laboratory for Reactive Chemistry on Solid Surfaces, Institute of Physical Chemistry, Zhejiang Normal University, Jinhua, 321004, Zhejiang, People’s Republic of China

    Xiao-Yong Zheng, Cai-Hong Zhan, Shu-Guang Zhang & Yun-Long Feng

Authors
  1. Xiao-Yong Zheng
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  2. Cai-Hong Zhan
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  3. Shu-Guang Zhang
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  4. Yun-Long Feng
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Corresponding author

Correspondence to Yun-Long Feng.

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Zheng, XY., Zhan, CH., Zhang, SG. et al. A New Microporous Hydrogen-Bonding Framework Constructed from 1-(4-Hydroxyphenyl)-5-Thioacetatetetrazole. J Chem Crystallogr 41, 587–590 (2011). https://doi.org/10.1007/s10870-010-9821-8

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  • DOI: https://doi.org/10.1007/s10870-010-9821-8

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