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Synthesis and Crystal Structure of New N,N′-Bis[1-(4-methoxyphenyl)-5-methyl-1H-1,2,3-triazole-4-carbonyl]hydrazide

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Abstract

The N,N′-bis[1-(4-methoxyphenyl)-5-methyl-1H-1,2,3-triazole-4-carbonyl]hydrazide 6 was synthesized from aryl triazole acids and its structure is established by MS, IR, and 1H NMR spectral data. Compound 6, C22H22N8O4, Mr = 462.48, crystallizes in the monoclinic space group P2(1)/c with unit cell parameters a = 15.3451(8), b = 8.6486(4), c = 16.8502(9) Å, α = 90.00, β = 95.731(2), γ = 90.00º, V = 2225.1(2) Å3, Z = 4, and Dx = 1.381 mg m−3. The final R was 0.0450. The four aromatic rings are close to linear because of N···H–N hydrogen bonds.

Index Abstract

Synthesis and crystal structures of N,N′-bis[1-(4-methoxyphenyl)-5-methyl-1H-1,2,3-triazole-4-carbonyl]hydrazide

Heng-Shan Dong, Yan-Fei, Wang, Hong-Ru Dong, Bin, Wang, Bin Quan

N,N′-Bis[1-(4-methoxyphenyl)-5-methyl-1H-1,2,3-triazole-4-carbonyl]hydrazide was synthesized.

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Acknowledgements

The authors wish to acknowledge that this project is supported by Lanzhou University SKLAOC.

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Authors and Affiliations

  1. State Key Laboratory of Applied Organic Chemistry, Institute of Organic Chemistry, College of Chemistry and Chemical Engineering, Lanzhou University, Lanzhou, Gansu, 730000, China

    Heng-Shan Dong, Yan-Fei Wang & Bin Wang

  2. College of Science and Engineering, Gansu Association University, Lanzhou, Gansu, 730000, China

    Hong-Ru Dong, Bin Wang & Bin Quan

Authors
  1. Heng-Shan Dong
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  2. Yan-Fei Wang
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  3. Hong-Ru Dong
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  4. Bin Wang
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  5. Bin Quan
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Correspondence to Heng-Shan Dong.

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Dong, HS., Wang, YF., Dong, HR. et al. Synthesis and Crystal Structure of New N,N′-Bis[1-(4-methoxyphenyl)-5-methyl-1H-1,2,3-triazole-4-carbonyl]hydrazide. J Chem Crystallogr 39, 91–94 (2009). https://doi.org/10.1007/s10870-008-9421-z

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  • DOI: https://doi.org/10.1007/s10870-008-9421-z

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