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Crystal Structure of N-(tert-Butyl)-1-(3,5-dioxo-2-phenyltetrahydro-4-isoxazolyl)cyclohexane Carboxamide

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Abstract

The crystal structure of N-(tert-butyl)-1-(3,5-dioxo-2-phenyltetrahydro-4-isoxazolyl)-cyclohexane-carboxamide 1 has been determined. The title compound crystallized in the orthorhombic space group pbca with cell parameters, a = 10.6556(6) Å, b = 18.0132(11) Å, c = 19.5513(12) Å, v = 3752.7(4) Å3, Z = 8, D cal = 1.269 Mg/m3 at T = 120 K. The structure refined by full-matrix least-squares procedures to find R 1 = 0.0463 and wR 2 = 0.0937 for 3059 reflections. The soxazole ring isn’t coplanar with the phenyl ring.

Index Abstract

The crystal structure of N-(tert-butyl)-1-(3,5-dioxo-2-phenyltetrahydro-4-isoxazolyl)-cyclohexane-carboxamide 1 has been studied.

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Authors and Affiliations

  1. Faculty of Chemistry, Tarbiat Moallem University, 49 Mofatteh Avenue, Tehran, Iran

    Azizollah Habibi & Leyla Mousavifar

  2. Chemistry Department, Guilan University, Rasht, Guilan, Iran

    Mohammad R. Yazdanbakhsh & Leyla Mousavifar

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  1. Azizollah Habibi
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  2. Mohammad R. Yazdanbakhsh
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  3. Leyla Mousavifar
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Correspondence to Azizollah Habibi.

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Habibi, A., Yazdanbakhsh, M.R. & Mousavifar, L. Crystal Structure of N-(tert-Butyl)-1-(3,5-dioxo-2-phenyltetrahydro-4-isoxazolyl)cyclohexane Carboxamide. J Chem Crystallogr 38, 701–704 (2008). https://doi.org/10.1007/s10870-008-9379-x

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  • DOI: https://doi.org/10.1007/s10870-008-9379-x

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