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Structure of 6,13-bis(N, N-dimethylcarbamoyl) thioquinanthrene

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The crystal structure of 6,13-bis-(N,N-dimethylcarbamoyl)thioquinanthrene 3 has been determined as monoclinic, with space group P2(1)/c with lattice parameters a = 10.044(2) Å, b = 21.385(4) Å, c = 10.889(3) Å, β = 102.92(3)°, Z = 4 and Dcalc = 1.342 Mg/m3. The middle 1,4-dithiin ring in the title compound 3, C24H20N4O2S2 is in a boat conformation with the dihedral angle between the planes of the aromatic rings 132.45(8)°.

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References

  • Maślankiewicz, A.; Michalik, E.; Głowiak T. J. Chem. Crystallogr. 1998, 28, 35.

    Google Scholar 

  • Michalik, E. 2001. Doctoral Disertation, University of Wrocław, procław, (Poland).

  • Lynch, S. B.; Simonsen, S. H.; Davis, B. E. Acta Cryst. 1994, C50, 1470.

    Google Scholar 

  • Pignedoli, A.; Peyronel, G.; Antolini, L. J. Cryst. Mol. Struct. 1977, 7, 173.

    Google Scholar 

  • Larson, S. B.; Simonsen, S. H.; Martin, G. H.; Smith, K.; Puig-Torres, S. Acta Cryst. 1984, C40, 103.

    Google Scholar 

  • 6 Maślankiewicz, A.; Michalik, E. J. Heterocyclic Chem. 1997, 34, 401.

    Google Scholar 

  • Sheldrick, G. M. Acta Cryst. 1990, A46, 467.

    Google Scholar 

  • Sheldrick, G. M. 1997, Program for the Refinement of Crystal Structure, University of Göttingen, Germany.

    Google Scholar 

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Authors and Affiliations

  1. Department of Organic Chemistry, The Medical University of Silesia Jagiellońska 4, 41-200, Sosnowiec, Poland

    Andrzej Maślankiewicz & Ewa Michalik

  2. Institute of Chemistry, University of Wrocław, F.Joliot-Curie 14, 50-383, Wrocław, Poland

    Tadeusz Głowiak

  3. Oxford Diffraction, ul. Rogowska 127A, 54-440, Wrocław, Poland

    Andrzej Kowalski

Authors
  1. Andrzej Maślankiewicz
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  2. Ewa Michalik
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  3. Tadeusz Głowiak
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  4. Andrzej Kowalski
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Correspondence to Andrzej Maślankiewicz.

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Maślankiewicz, A., Michalik, E., Głowiak, T. et al. Structure of 6,13-bis(N, N-dimethylcarbamoyl) thioquinanthrene. J Chem Crystallogr 34, 825–828 (2004). https://doi.org/10.1007/s10870-004-7714-4

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  • DOI: https://doi.org/10.1007/s10870-004-7714-4

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