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Relationship between structural and magnetic properties of 48Ni–52Fe laminates: improvement study induced by annealing conditions

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Abstract

48Ni–52Fe laminates are useful in many applications, especially in stepper motors, watches, relays, transformers, etc. This paper presents an evolution of the microstructural and magnetic properties of 48Ni–52Fe alloy in the form of laminates treated under different annealing conditions. The relationship of microstructure, heat treatment parameters (annealing and surface oxidation), saturation magnetization (Ms), and coercivity (Hc) is established. FCC crystalline structure with considerably large grains was observed after the annealing (1050 °C, 2 h) with significantly increased grain size. Magnetic characterization revealed that after applying heat treatment, a significant improvement of saturation magnetization along with a decrease in coercivity value was observed. Post-annealing oxidation treatment (400 °C, 2 h), helped to improve the hardness of the samples; however, a slight decrease in the magnetic properties was observed.

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Acknowledgements

The authors are also thankful to Shri. R. S. Shinde, Former OS and Head, AMTD, RRCAT, Indore for fruitful discussions during the work.

Funding

The authors acknowledge Board of Research in Nuclear Sciences (BRNS), Government of India, for financial funding through the research grant no.59/14/07/2019-BRNS/34105.

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Authors and Affiliations

  1. Centre for Materials for Electronics Technology (C-MET), Panchawati, Off. Dr. Bhabha Road, Pune, 411007, India

    Shubhangi Supekar, Rahul Ghuge, Manish Shinde & Sunit Rane

  2. Indian Institute of Technology (IIT), Mumbai, 400076, India

    Sanjay Manda

  3. Raja Ramanna Centre for Advanced Technology (RRCAT), Indore, 452013, India

    S. Senthil Kumar & Prashant Pareek

Authors
  1. Shubhangi Supekar
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  2. Rahul Ghuge
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  5. S. Senthil Kumar
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  6. Prashant Pareek
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  7. Sunit Rane
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Contributions

Shubhangi Supekar contributed to Conceptualization, Methodology, Investigation, Formal analysis, Writing of the Original draft, and Visualization. Rahul Ghuge contributed to Magnetic measurements and Formal analysis, Manish Shinde contributed to Validation, Formal analysis, Resources, Supervision, and Writing, Reviewing & Editing of the manuscript , Sanjay Manda contributed to EBSD analysis, S. Senthil Kumar contributed to Resources and material support. Prashant Pareek contributed to Resources and material support. Sunit B Rane contributed to Writing, Reviewing, and Editing of the manuscript, Formal analysis, Resources, Supervision, and Project administration.

Corresponding authors

Correspondence to Manish Shinde or Sunit Rane.

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Supekar, S., Ghuge, R., Shinde, M. et al. Relationship between structural and magnetic properties of 48Ni–52Fe laminates: improvement study induced by annealing conditions. J Mater Sci: Mater Electron 35, 518 (2024). https://doi.org/10.1007/s10854-024-12260-w

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