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An industrial feasible and sustainable method for preparing fiberized bamboo-derived magnetic biomass carbon

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Abstract

With the progress of science and technology and the improvement of people’s living standards, the high-value utilization of waste bamboo materials and the increasingly serious problem of electromagnetic wave (EMW) pollution have attracted more and more attention. The above two problems can be solved simultaneously by overcoming the structural defects of bamboo, such as dense arrangement of fiber cells, horizontal gradient stratification and so on, realizing the impregnation of inorganic materials, and then obtaining magnetic biochar-based EMW absorbers by in situ pyrolysis. Here, we carry out fibrosis treatment to obtain bamboo bundles with significantly increased specific surface area and a large number of exposed inner walls of fiber cells. After that, the bamboo bundles are impregnated in iron acetylacetonate (Fe(acac)3) DMF solution with concentrations of 0.04, 0.08 and 0.12 g/mL, and fiberized bamboo-derived magnetic biomass carbon (FBMC) are finally prepared through in situ pyrolysis technology. The results show that the EMW absorption performance of the prepared FBMCs is best with an impregnation concentration of 0.04 g/mL, and the minimum reflection loss is − 28.21 dB at 13.40 GHz with a matching thickness of 3 mm. With further increase of the impregnation concentration, the magnetic properties and electrical conductivities of FBMCs are enhanced, but their corresponding EMW absorption performance is deteriorated. Further research shows that the absorption capacities mainly come from the good dielectric loss caused by the interfacial polarization effect, and the magnetic loss caused by natural and exchange response. It is proved that the attenuation ability of FBMC-0.04 to EMW energy mainly comes from EMW absorption behavior.

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Funding

This research was funded by financial support from the National Natural Science Foundation of China (No. 31971740), Jiangsu Agricultural Science and Technology Independent Innovation Fund (CX (20)3041), Open Fund of Key Laboratory of National Forestry and Grassland Administration/Beijing for Bamboo & Rattan Science and Technology (ICBR-2020-08).

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Authors and Affiliations

  1. Jiangsu Co-Innovation Center of Efficient Processing and Utilization of Forest Resources, Nanjing Forestry University, Nanjing, 210037, China

    Feng Yuan & Lou Zhichao

  2. College of Materials Science and Engineering, Nanjing Forestry University, Nanjing, 210037, China

    Feng Yuan, Sun Wei, Lou Zhichao, Wang Qiuyi, Zhao Yihan & Li Yanjun

  3. Bamboo Engineering and Technology Research Center, State Forestry and Grassland Administration, Nanjing, 210037, China

    Lou Zhichao & Li Yanjun

  4. Key Laboratory of National Forestry and Grassland Administration/Beijing for Bamboo & Rattan Science and Technology, Beijing, 100102, China

    Lou Zhichao

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  1. Feng Yuan
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  2. Sun Wei
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  3. Lou Zhichao
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  4. Wang Qiuyi
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  5. Zhao Yihan
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Contributions

FY and SW prepared the samples, and analyzed and interpreted the obtained results. WQ and ZY performed the SEM, XRD, XPS, Raman and VSM characterizations. FY performed the electromagnetic characteristics and calculated the relevant parameters of electromagnetic wave absorption. FY and SW are major contributors in writing the manuscript. LZ and LY design the experiments and help to analyze the data. All authors read and approved the final manuscript.

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Correspondence to Lou Zhichao or Li Yanjun.

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Yuan, F., Wei, S., Zhichao, L. et al. An industrial feasible and sustainable method for preparing fiberized bamboo-derived magnetic biomass carbon. J Mater Sci: Mater Electron 32, 26137–26150 (2021). https://doi.org/10.1007/s10854-021-06498-x

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