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Modified polyacrylamide gel synthesis of CeO2 nanoparticles by using cerium sulfate as metal source and its optical and photoluminescence properties

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Abstract

Developing a novel method to synthesize the highly dispersed nanosemiconductor materials is the major challenge in the expand the application field of luminescent materials. A modified polyacrylamide gel method has been used to synthesize the CeO2 nanoparticles by using cerium sulfate as metal source. The method makes full use of exothermic reaction of cerium sulfate in the precursor solution to polymerize acrylamide and methylene diacrylamide to obtain gel. The phase purity, particle size, optical properties, and photoluminescence properties of CeO2 nanoparticles demonstrate the strongly dependent behavior of acrylamide and methylene diacrylamide (AMMD) content. The synergistic effect of oxygen vacancy concentration, impurity functional group, and surface adsorbed oxygen leads to high photoluminescence performance of CeO2 nanoparticles prepared with the AMMD content of 0.3.

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Funding

This work was supported by the Project 2019DB02 supported by NPL, CAEP, the Science and Technology Research Program of Chongqing Education Commission of China (KJZD-K202001202, KJQN201901), the NSAF joint Foundation of China (U2030116), the Chongqing Natural Science Foundation (cstc2019jcyj-msxmX0310), the Talent Introduction Project (09924601), Major Cultivation Projects (18ZDPY01), and Research Project of Higher Education Teaching Reform (JGZC1903) of Chongqing Three Gorges University.

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  1. School of Electronic and Information Engineering, Chongqing Three Gorges University, Wanzhou, 404000, Chongqing, China

    Shifa Wang, Shengnan Tang, Huajing Gao, Xiangyu Chen, Chuan Yu, Hao Liu & Xudong Pan

  2. Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang, 621900, Sichuan, China

    Leiming Fang, Qiwei Hu & Guangai Sun

  3. State Key Laboratory of Advanced Processing and Recycling of Non-ferrous Metals, Lanzhou University of Technology, Lanzhou, 730050, Gansu, China

    Huajing Gao

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SW involved in experiment, data analysis and paper writing, and supervision and paper revision. HG and LF performed supervision. ST did experimental test and analysis. QH, GS, XC, CY, HL, and XP performed writing- reviewing and editing.

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Wang, S., Tang, S., Gao, H. et al. Modified polyacrylamide gel synthesis of CeO2 nanoparticles by using cerium sulfate as metal source and its optical and photoluminescence properties. J Mater Sci: Mater Electron 32, 10820–10834 (2021). https://doi.org/10.1007/s10854-021-05740-w

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