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Facile preparation of graphene oxide for low-κ epoxy nanocomposites with improved thermal stability

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Abstract

The graphene and graphene oxide have drawn much attention due to their excellent physical and chemical performances, as well as 2-dimension structure and high surface area. Herein, a facile method was proposed to prepare the graphene oxide and it was then introduced into epoxy to prepare nanocomposites. Results showed that the dielectric constant of the epoxy/graphene oxide nanocomposite was decreased by adding only 0.2 wt% of the fillers, while the dielectric loss stayed at a low level. Meanwhile, the glass-transition temperature of the nanocomposite was increased to 90.3 °C from 74.9 °C for the pure epoxy. Moreover, the thermal decomposition temperature (at 5% weight loss) of the nanocomposite was also increased greatly. Based on these results, we suggested that the graphene oxide was a promising additive for preparing low-κ epoxy nanocomposites with high properties.

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Acknowledgements

This study was supported by the financial supports from the National Natural Science Foundation of China (Grant Nos. 51403013, 51273017, 20974013).

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Authors and Affiliations

  1. State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, People’s Republic of China

    Yongke Zhao, Guomin Song, Zheng Zhou & Qifang Li

  2. Key Laboratory of Carbon Fiber and Functional Polymers, Ministry of Education, Beijing University of Chemical Technology, Beijing, 100029, People’s Republic of China

    Guangxin Chen

  3. College of Materials Science and Engineering, Beijing University of Chemical Technology, Beijing, 100029, People’s Republic of China

    Yongke Zhao, Guomin Song, Guangxin Chen, Zheng Zhou & Qifang Li

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  1. Yongke Zhao
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  2. Guomin Song
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Correspondence to Qifang Li.

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Zhao, Y., Song, G., Chen, G. et al. Facile preparation of graphene oxide for low-κ epoxy nanocomposites with improved thermal stability. J Mater Sci: Mater Electron 31, 310–316 (2020). https://doi.org/10.1007/s10854-019-02515-2

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  • DOI: https://doi.org/10.1007/s10854-019-02515-2

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