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Synthesis and characterization of II–VI (CdSe) quantum dot encapsulated liposomes

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Abstract

The semiconductor CdSe quantum dots (QDs) with emission spectra of different wavelengths were synthetized by using a modified method of simultaneous injection at heating. The obtained QDs were encapsulated into liposomes prepared by a method of lipid film hydration and sonication from various phospholipid compositions and polyethylene glycol (PEG) addition. The synthesized and encapsulated in the liposomes QDs were characterized by photoluminescence (PL), X-Ray diffraction (XRD), Transmission electron microscopy, and Dynamic light scattering. The evaluation of PL spectra of the obtained QDs showed that they had sizes in the range of 2.3–4.5 nm. XRD patterns revealed only one peak for CdSe cubic crystal structure and the estimated crystal sizes were about the same values that the obtained from PL results. After the encapsulation a blue shift of PL peak position was observed. The mechanism of the effect is discussed.

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Acknowledgements

The work was partially supported by project of SIP and CNMN of Instituto Politécnico Nacional (Mexico), as well as Laboratory of Elemental Particles of the Department of Physics of CINVESTAV. The authors kindly thank Anton Paar México S.A. de C.V. for the DLS measurements.

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Authors and Affiliations

  1. UPIITA – Instituto Politécnico Nacional, Othón de Mendizábal S/N, La Escalera, 07320, Mexico City, Mexico

    J. Douda & L. G. Miranda Calderón

  2. Instituto Politécnico Nacional, ESFM, Departamento de Física, U.P.A.L.M., Av. IPN S/N, Edif. 9, CP 07738, Mexico City, Mexico

    T. Kryshtab

  3. CINVESTAV-IPN, Solid State Electronics Section, Department of Electrical Engineering, Av. Instituto Politécnico Nacional, 2508, San Pedro Zacatenco, C.P. 07360, Mexico City, Mexico

    J. S. Arias Cerón

  4. Instituto Politécnico Nacional, ESIME - Zacatenco, Departamento de Sistemas, U.P.A.L.M., Av. IPN S/N, Edif. Z-4, CP 07738, Mexico City, Mexico

    A. Kryvko

  5. UPIITA, Instituto Politécnico Nacional, 07340, Mexico City, Mexico

    J. Douda

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  1. J. Douda
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  2. L. G. Miranda Calderón
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  3. T. Kryshtab
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  4. J. S. Arias Cerón
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  5. A. Kryvko
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Correspondence to J. Douda.

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Douda, J., Miranda Calderón, L.G., Kryshtab, T. et al. Synthesis and characterization of II–VI (CdSe) quantum dot encapsulated liposomes. J Mater Sci: Mater Electron 29, 15570–15578 (2018). https://doi.org/10.1007/s10854-018-9133-x

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  • DOI: https://doi.org/10.1007/s10854-018-9133-x

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