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Novel synthesis method for photo-catalytic system based on some 3d-metal titanates

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Abstract

In this paper, we studied titanium (TiO2) nanoparticle in three different structures (Anatase, Rutile, and Degussa) and then they were synthesized by the sol–gel method which is used butanol, toluene, and triethylene glycol as solvent at different temperatures and times. Then in this case to modify the TiO2, doping was done by transition metals and CdTiO3, CrTiO3, NiTiO3, MnTiO3, FeTiO3, and CoTiO3 were synthesized. The pure MTiO3 (M = Cd, Cr, Ni, Mn, Fe and Co) nanoparticles were formed when the precursor was heat-treated at 750 °C for 210 min. Characterizing the new additions was conducted by X-ray diffraction, FT-IR spectroscopy, UV–Vis spectroscopy, Scanning electron microscopy (SEM) image and N2 absorption–desorption. The BET analysis was performed to calculate the specific surface area. Pore diameter, pore volume, and the percentage of mesoporous MTiO3 were obtained by the BJH method according to the reaction. Titanium(IV) butoxide as a precursor was reacted with the metals and the energy band gap based on the metals decreased markedly and differently. To show the existing bond of titanium and metals, FT-IR and SEM image were used to investigate the obtained addition and investigating better their morphology respectively. To evaluate the photocatalytic properties of the nanocrystalline TiO2 (Degussa P-25) and MTiO3, the photocatalytic degradation of salicylic acid as a chemical toxic compound under ultraviolet light irradiation was carried out.

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  • 07 October 2017

    The original version of this article unfortunately contained an error in one of the co-author’s name. The third author’s name should read as “Nikolai N. Lobanov” instead of “Nikolay N.Lobanovc”.

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Funding

This work was supported by the Ministry of Education and Science of Russian Federation on the program to improve the competitiveness of People’s Friendship University of Russia (RUDN University) among the world’s leading research and education centers in 2016–2020. [Grant Number 02.a03.0008].

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Authors and Affiliations

  1. General Chemistry Department, RUDN University, 6 Miklukho-Maklaya st., Moscow, Russia, 117198

    Yahya Absalan & Olga V. Kovalchukova

  2. Physical and Colloidal Chemistry Department, RUDN University, 6 Miklukho-Maklaya st., Moscow, Russia, 117198

    Irena G. Bratchikova

  3. Inorganic Chemistry Department, RUDN University, 6 Miklukho-Maklaya st., Moscow, Russia, 117198

    Nikolai N. Lobanov

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  1. Yahya Absalan
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  2. Irena G. Bratchikova
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  3. Nikolai N. Lobanov
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  4. Olga V. Kovalchukova
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Correspondence to Yahya Absalan.

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The original version of this article was revised: The third author name was incorrect. This has been corrected in this version.

A correction to this article is available online at https://doi.org/10.1007/s10854-017-7879-1.

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Absalan, Y., Bratchikova, I.G., Lobanov, N.N. et al. Novel synthesis method for photo-catalytic system based on some 3d-metal titanates. J Mater Sci: Mater Electron 28, 18207–18219 (2017). https://doi.org/10.1007/s10854-017-7769-6

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