Abstract
Honeycomb-shaped and ordered arrays of nanopore AAO template with a uniform pores size was produced utilizing a two-step an anodization process. Highly ordered SnO2 nanorods arrays have been selectively fabricated via a convenient (immerse and filtration) technique and (vacuum and drop) setting using anodic aluminum oxide (AAO) as a hard template. The morphology of the samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (FESEM), and Energy-dispersive X-ray spectroscopy (EDX) techniques. The optical characterizations were examined by UV-VIS and Photoluminescence (PL). Scanning microscopy images indicate that the SnO2 nanorods are relatively uniform with the outer diameter matching well with the pore diameter. XRD and EDX indicated that these polycrystalline SnO2 nanostructures with well-defined composition were obtained.
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J. Ye, Hu Zhang, Yang Ro, X. Li, L. Qi, Morphology-controlled synthesis of SnO2 nanotubes by using 1D silica mesostructures as sacrificial templates and their applications in lithium-ion batteries. Small 6(2), 296–306 (2010)
Q. Chen, W.Z. Zhou, G.H. Du, L.M. Peng, Tritanate nanotubes made via a single alkali treatment. Adv. Mater. 14(17), 1208–1211 (2002)
J. Pan, H. Shen, and S. Mathur, One-dimensional SnO2 nanostructures: synthesis and applications. J Nanotechnol. Article ID 917320, 1–12 (2011)
W. Zhu, W. Wang, H. Xu, J. Shi, Fabrication of ordered SnO2 nanotube arrays via a template route. Mater. Chem. Phys. 99(1), 127–130 (2006)
L. Shi, Y. Xu, Q. Li, Controlled fabrication of SnO2 arrays of well-aligned nanotubes and nanowires. The Royal Soc. Chem. Nanoscale. 2, 2104–2108 (2010)
C.C. Tsai, H. Teng, Regulation of the physical characteristics of titania nanotube aggregates synthesized from hydrothermal treatment. Chem. Mater. 16(22), 4352–4358 (2004)
J.Q. Hu, X.L. Ma, N.G. Shang, Z.Y. Xie, N.B. Wong, C.S. Lee, S.T. Lee, Large-scale rapid oxidation synthesis of SnO2 nanoribbons. J. Phys. Chem. B 106(15), 3823–3826 (2002)
J.Q. Hu, Y. Bando, Q.L. Liu, D. Golberg, Laser-ablation growth and optical properties of wide and long single-crystal SnO2 ribbons. Adv. Funct. Mater. 13(6), 493–496 (2003)
D. Calestani, L. Lazzarini, G. Salviati, M. Zha, Morphological structural and optical study of quasi-1D SnO2 nanowires and nanobelts. Cryst. Res. Technol. 40(10–11), 937–941 (2005)
G. Faglia, C. Baratto, G. Sberveglieri, M. Zha, A. Zappettini, Adsorption effects of NO2 at ppm level on visible photoluminescence response of SnO2 nanobelts. Appl. Phys. Lett. 86(1), 011923 (2005)
D. Cai, Y. Su, Y. Chen, J. Jiang, Z. He, L. Chen, Synthesis and photoluminescence properties of Nnvel of SnO2 asterisk-like nanostructures. Mater. Lett. 59(16), 1984–1988 (2005)
D. Maestre, A. Cremades, J. Piqueras, Growth and luminescence properties of micro-and nanotubes in sintered tin oxide. J. Appl. Phys. 97(4), 044316 (2005)
D.F. Cox, T.B. Fryberger, S. Semancik, Oxygen vacancies and defect electronic states on the SnO2 (110)−1 x 1 surface. Phys. Rev. B 38(3), 2072–2083 (1988)
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Sabry, R.S., Alobaidi, R. Template assisted synthesis of SnO2 nanorods by immerse and filtration technique, vacuum and drop setting. J Mater Sci: Mater Electron 27, 10036–10044 (2016). https://doi.org/10.1007/s10854-016-5075-3
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DOI: https://doi.org/10.1007/s10854-016-5075-3