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Preparation of Li2MoO4 using aqueous solution method and microwave dielectric properties after sintering

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Abstract

A novel aqueous solution method was used to prepare Li2MoO4 powder, which was pressed and sintered directly into ceramic pellets without any calcination or milling stage involved. Pure Li2MoO4 ceramic with the maximum bulk density of 2.898 g/cm3 (95.63 % of the theoretical value) and excellent microwave dielectric properties of ɛ r  = 5.58, Q × f = 49,328 GHz, τf = −168 ppm/°C (f = 10.17 GHz) was obtained at 540 °C/2 h. The maximum Q × f value in this work is higher than that of Li2MoO4 ceramic prepared by the conventional solid-state reaction method. The results show that the aqueous solution method is a simple and effective method to produce Li2MoO4 ceramics.

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References

  1. H.H. Xi, D. Zhou, H.D. Xie, W.B. Li, Mater. Lett. 142, 221–224 (2015)

    Article  Google Scholar 

  2. D. Zhou, L.X. Pang, J. Guo, Z.M. Qi, T. Shao, Q.P. Wang, H.D. Xie, X. Yao, C.A. Randall, Inorg. Chem. 53(2), 1048–1055 (2014)

    Article  Google Scholar 

  3. D.K. Kwon, M.T. Lanagan, T.R. Shrout, J. Am. Ceram. Soc. 88(12), 3419–3422 (2005)

    Article  Google Scholar 

  4. M. Valant, D. Suvorov, J. Am. Ceram. Soc. 83(11), 2721–2729 (2000)

    Article  Google Scholar 

  5. D. Zhou, H. Wang, X. Yao, L.X. Pang, J. Am. Ceram. Soc. 91(10), 3419–3422 (2008)

    Article  Google Scholar 

  6. D. Zhou, H. Wang, L.X. Pang, C.A. Randall, X. Yao, J. Am. Ceram. Soc. 92(10), 2242–2246 (2009)

    Article  Google Scholar 

  7. G. Subodh, M.T. Sebastian, J. Am. Ceram. Soc. 90(7), 2266–2268 (2007)

    Article  Google Scholar 

  8. G.K. Choi, J.R. Kim, S.H. Yoon, K.S. Hong, J. Eur. Ceram. Soc. 27, 3063–3067 (2007)

    Article  Google Scholar 

  9. J. Guo, D. Zhou, S.L. Zou, H. Wang, L.X. Pang, X. Yao, J. Am. Ceram. Soc. 97(6), 1819–1822 (2014)

    Article  Google Scholar 

  10. D. Zhou, L.X. Pang, Z.M. Qi, B.B. Jin, X. Yao, Sci. Rep. 4, 5980 (2014)

    Google Scholar 

  11. J. Honkamo, H. Jantunen, G. Subodh, M.T. Sebastian, P. Mohanan, Int. J. Appl. Ceram. Tec. 6(4), 531–536 (2009)

    Article  Google Scholar 

  12. D. Zhou, C.A. Randall, L.X. Pang, H. Wang, X.G. Wu, J. Guo, G.Q. Zhang, L. Shui, X. Yao, J. Am. Ceram. Soc. 94(3), 802–805 (2011)

    Article  Google Scholar 

  13. D. Zhou, C.A. Randall, H. Wang, L.X. Pang, X. Yao, J. Am. Ceram. Soc. 93(4), 1096–1100 (2010)

    Article  Google Scholar 

  14. B.W. Hakki, P.D. Coleman, I.E.E.E. Trans, Microw. Theory Tech. 8, 402–410 (1960)

    Article  Google Scholar 

  15. L.X. Li, J. Ye, S. Zhang, Z.D. Gao, S. Li, J. Alloys Compd. 648, 184–189 (2015)

    Article  Google Scholar 

  16. X.M. Chen, Y. Suzuki, N. Sato, J. Mater. Sci.: Mater. Electron. 6(1), 10–16 (1995)

    Google Scholar 

  17. C.-S. Hsu, C.-L. Huang, J.-F. Tseng, C.-Y. Huang, Mater. Res. Bull. 38(6), 1091–1099 (2003)

    Article  Google Scholar 

  18. I.M. Reaney, D. Iddles, J. Am. Ceram. Soc. 89(7), 2063–2072 (2006)

    Google Scholar 

  19. D. Zhou, C.A. Randall, L.X. Pang, H. Wang, J. Guo, G.Q. Zhang, J. Am. Ceram. Soc. 94(2), 348–350 (2011)

    Article  Google Scholar 

  20. G.K. Choi, S.Y. Cho, J.S. An, K.S. Hong, J. Eur. Ceram. Soc. 26, 2011–2015 (2006)

    Article  Google Scholar 

  21. S.H. Yoon, D.W. Kim, S.Y. Cho, K.S. Hong, J. Eur. Ceram. Soc. 26, 2051–2054 (2006)

    Article  Google Scholar 

Download references

Acknowledgments

This work was financially sponsored by the Seed Foundation of Tianjin University and the National Natural Science Foundation of China (No. 61201038).

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Authors and Affiliations

  1. School of Electronic Information Engineering, Tianjin University, Tianjin, 300072, China

    Hao Zhang, Xiuyu Wang, Qiang Cheng, Xiaopin Ma, Mingxiu Li, Ping Zhang & Yonggui Zhao

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  1. Hao Zhang
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  2. Xiuyu Wang
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  3. Qiang Cheng
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  4. Xiaopin Ma
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  5. Mingxiu Li
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  6. Ping Zhang
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  7. Yonggui Zhao
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Correspondence to Xiuyu Wang.

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Zhang, H., Wang, X., Cheng, Q. et al. Preparation of Li2MoO4 using aqueous solution method and microwave dielectric properties after sintering. J Mater Sci: Mater Electron 27, 5422–5426 (2016). https://doi.org/10.1007/s10854-016-4444-2

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  • DOI: https://doi.org/10.1007/s10854-016-4444-2

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