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Microwave synthesis of CaSiO3:(Eu2+, Dy3+) nanorods and verification on luminescence properties

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Abstract

CaSiO3:(Eu2+, Dy3+) nanorods were synthesized by microwave irradiation process with assistant of polyethylene glycol (PEG)-1000. The X-ray diffraction results show that the obtained samples are of β-CaSiO3 phase with perovskite structure. The TEM images show that the obtained samples are of nanorods with diameter around 40 nm and length ranging from 0.6 to 1.2 μm. PEG-1000 plays an important role in the formation of claviform morphology. The excitation and emission spectra of CaSiO3:(Eu2+, Dy3+) samples show characteristic transitions of Eu2+ ions. All samples give a green emission peaked at 512 nm when they are excited at 366 nm. The co-doped Dy3+ ions enhance the luminescence intensity greatly but have no obvious influences on location of emission peak. CaSiO3:(0.05Eu2+, 0.03Dy3+) samples give the highest luminescence intensity.

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Authors and Affiliations

  1. Science and Technology on Reliability and Environmental Engineering Laboratory, Beijing, 100191, China

    Xiaoqi Xing, Dongyi Ling & Lin Tan

  2. School of Reliability and Systems Engineering, Beihang University, Beijing, 100191, China

    Xiaoqi Xing, Dongyi Ling & Lin Tan

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  1. Xiaoqi Xing
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  2. Dongyi Ling
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  3. Lin Tan
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Correspondence to Lin Tan.

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Xing, X., Ling, D. & Tan, L. Microwave synthesis of CaSiO3:(Eu2+, Dy3+) nanorods and verification on luminescence properties. J Mater Sci: Mater Electron 25, 4774–4778 (2014). https://doi.org/10.1007/s10854-014-2232-4

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  • DOI: https://doi.org/10.1007/s10854-014-2232-4

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