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Synthesis and magnetic properties of conventional and microwave calcined barium hexaferrite powder

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Abstract

Single phase nanoparticles of barium hexaferrite (BaFe12O19–BaF) were synthesized by sol–gel method using metal nitrates as source and d-Fructose as a fuel. The prepared precursors were calcined by two different calcination techniques, using conventional furnace and microwave furnace. The samples are characterized using powder X-ray diffraction, theromogravimetric analysis and vibration sample magnetometer. Thermal analysis studies showed exothermic and endothermic reaction peaks from room temperature to 1,200 °C. X-ray diffraction studies established the formation temperature of single phase BaFe12O19. HR-SEM results showed the dispersed particles of hexagonal structure in platelet form. The broad hysteresis loop showed that the barium hexaferrite powder was in good crystalline nature.

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References

  1. D. Lisijak, M. Drofenik, J. Eur. Ceram. Soc 27, 4515 (2007)

    Article  Google Scholar 

  2. M.M. Rashad, M. Radwan, M.M. Hessien, J. Alloys Comps. 453, 304 (2008)

    Article  CAS  Google Scholar 

  3. D. Mishra, S. Anand, R.K. Panda, R.P. Das, Mater. Chem. Phys. 86, 132 (2004)

    Article  CAS  Google Scholar 

  4. R.M. Garcia, E.R. Ruiz, E.E. Rams, R.M. Sanchez, J. Magn. Magn. Mater. 223, 133 (2001)

    Article  Google Scholar 

  5. P. Shepherd, K.K. Mallick, R.J. Green, J. Magn. Magn. Mater. 311, 683 (2007)

    Article  CAS  Google Scholar 

  6. Q. Mohsen, J. Alloys Comps. 500, 125 (2010)

    Article  CAS  Google Scholar 

  7. S. Ramesh, C.Y. Tan, S.B. Bhaduri, W.D. Teng, I. Sopyan, J. Mater. Process. Technol. 206, 221 (2008)

    Article  CAS  Google Scholar 

  8. A. Mondal, A. Upadhyaya, D. Agrawal, Mat. Sci. Eng. A 527, 6870 (2010)

    Article  Google Scholar 

  9. A. Ataie, S. Heshmatimanesh, H. Kazempour, J. Mat. Sci. 37, 2125 (2002)

    Article  CAS  Google Scholar 

  10. H. Shang, J. Wang, Q.F. Liu, Mat. Sci. Eng. A 456, 130 (2007)

    Article  Google Scholar 

  11. D.S. Patil, B.C. Mutsuddy, Ceramic Transactions 21, 301 (1991)

    CAS  Google Scholar 

  12. Z. Xie, Z. Gui, L. Li, X. Huang, Y. Huang, J. Mat. Sci. 35, 203 (2000)

    Article  CAS  Google Scholar 

  13. M.C.L. Patterson, R.M. Kimber, P.S. Apte, in Microwave Processing of Materials II, ed. by B. Snyder, W.H. Sutton, M.F. Iskander, D.L. Johnson, Mater. Res. Soc. Symp. Proc 189, 257 (1990)

  14. X. Tang, B.Y. Zhao, K.A. Hu, J. Mat. Sci. 41, 3867 (2006)

    Article  CAS  Google Scholar 

  15. J. Dho, E.K. Lee, J.Y. Park, N.H. Hur, J. Magn. Magn. Mater. 285, 164 (2005)

    Article  CAS  Google Scholar 

  16. P. Ren, J.G. Guan, X.D. Cheng, Mater. Chem. Phys. 98, 90 (2006)

    Article  CAS  Google Scholar 

  17. S. Kanagesan, S. Jesurani, R. Velmurugan, C. Kumar, T. Kalaivani, J. Mat. Sci. Eng. 4, 88 (2010)

    Google Scholar 

  18. R. Ramesh, K. Ashok, G.M. Bhalero, S. Ponnusamy, C. Muthamizhchelvan, Cyst. Res. Technol. 45, 956 (2010)

    Google Scholar 

Download references

Acknowledgments

The authors thank SRM University for providing the facilities available in Nanotechnology center.

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Authors and Affiliations

  1. Center for Material Science and Nano Devices, Department of Physics, SRM University, Kattankulathur, Tamil Nadu, 603 203, India

    S. Kanagesan, S. Jesurani, R. Velmurugan, M. Sivakumar, C. Thirupathi & T. Kalaivani

  2. Department of Physics, Jeyaraj Annapackium College for Women, Periyakulam, Tamil Nadu, 625 601, India

    S. Jesurani

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  1. S. Kanagesan
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  2. S. Jesurani
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  3. R. Velmurugan
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  4. M. Sivakumar
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  6. T. Kalaivani
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Correspondence to S. Kanagesan.

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Kanagesan, S., Jesurani, S., Velmurugan, R. et al. Synthesis and magnetic properties of conventional and microwave calcined barium hexaferrite powder. J Mater Sci: Mater Electron 23, 635–639 (2012). https://doi.org/10.1007/s10854-011-0460-4

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  • DOI: https://doi.org/10.1007/s10854-011-0460-4

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