Journal of Materials Science

, Volume 53, Issue 17, pp 12492–12503 | Cite as

Biaxial fatigue property enhancement of gradient ultra-fine-grained Zircaloy-4 prepared by surface mechanical rolling treatment

  • Chao Xin
  • Qiaoyan Sun
  • Lin Xiao
  • Jun Sun


Surface mechanical rolling treatment (SMRT) was applied to modify the microstructure and biaxial fatigue properties of Zircaloy-4 tubes. Gradient ultra-fine microstructural layers of ~ 500 μm in-depth from the outside surface were fabricated on rods. Residual compressive stresses with gradient distribution were simultaneously produced. Biaxial tension–torsion fatigue test was conducted to assess the effect of modified microstructures and residual stress on the fatigue lifetime and deformed substructure of Zircaloy-4. The results show that the SMRT Zircaloy-4 alloy possesses more than double biaxial fatigue lifetime than that of the as-received Zircaloy-4 without SMRT at a tension–torsion stress ratio of 1.0. Microstructural examination reveals that the SMRT Zircaloy-4 alloy shows sequential deformation characteristics at different layers across the tubular wall during biaxial fatigue. The fatigued dislocation configuration changes from dislocation cells within the depth of 200 μm, to bent lamellar structures at the depth of ~ 300 μm, and embryonic dislocation cells at the depth of ~ 500 μm. The enhancement of biaxial fatigue life in the SMRT Zircaloy-4 can be attributed to the combined effects of the gradient ultra-fine structure and the gradient residual compressive stress in the vicinity of surface suppress the fatigue crack initiation and propagation.



This project was financially supported by the National Natural Science Foundation of China (51471129, 51671158, 51621063), 973 Program of China (2014CB644003), and the 111 Project of China (B06025).

Compliance with ethical standards

Conflict of interest

The authors declare that there is no conflict of interests regarding the publication of this article.


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© Springer Science+Business Media, LLC, part of Springer Nature 2018

Authors and Affiliations

  1. 1.State Key Laboratory for Mechanical Behavior of MaterialsXi’an Jiaotong UniversityXi’anPeople’s Republic of China

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