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Effect of annealing on microstructure and texture evolution of uniaxial hot compressed Mg–Al–Sn alloys

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Abstract

In this study, effects of dynamically formed precipitates on the microstructure and texture evolution were investigated during the post-deformation annealing. Two ternary alloys of Mg, Al, and Sn were produced and deformed at 250 and 300 °C to form different amounts of strain-induced precipitates during deformation and different levels of dynamic recrystallization. Subsequent annealing at deformation temperatures was performed at various times for up to 4 h and recrystallization, grain coarsening, and precipitation behaviors were characterized. The deformed structures were all partially dynamically recrystallized exhibiting necklacing. Static recrystallization (SRX) progressed by the transformation of the coarse grained un-necklaced regions to fine grains. It was found that increasing levels of pre-existing precipitates on dynamic recrystallized grain boundaries inhibited SRX as well as grain coarsening, by precipitation pinning. Texture was weakened after a short time annealing compared to the as-deformed condition and high amount of precipitates at the grain boundary restricted the grain coarsening and kept the texture weaken associated with grain coarsening.

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References

  1. Avedesian MM, Baker H (1999) ASM specialty handbook: magnesium and magnesium alloys. ASM International, Materials Park

    Google Scholar 

  2. Bettles C, Barnett M (2012) Advances in wrought magnesium alloys: fundamentals of processing, properties and applications. Woodhead Publishing Limited, Cambridge

    Book  Google Scholar 

  3. Kabir ASH, Sanjari M, Su J, Jung I-H, Yue S (2014) Effect of strain-induced precipitation on dynamic recrystallization in Mg–Al–Sn alloys. Mater Sci Eng, A 616:252–259

    Article  Google Scholar 

  4. Yang X, Miura H, Sakai T (2005) Isochronal annealing behavior of magnesium alloy AZ31 after hot deformation. Mater Trans 46:2981–2987

    Article  Google Scholar 

  5. Humphreys FJ, Hatherly M (2004) Recrystallization and related annealing phenomena, 2nd edn. Elsevier, Oxford

    Google Scholar 

  6. Huang X, Suzuki K, Chino Y (2013) Different annealing behaviours of warm rolled Mg–3Al–1Zn alloy sheets with dynamic recrystallized microstructure and deformation microstructure. Mater Sci Eng, A 560:232–240

    Article  Google Scholar 

  7. Su CW, Lu L, Lai MO (2008) Recrystallization and grain growth of deformed magnesium alloy. Philos Mag 88:181–200

    Article  Google Scholar 

  8. Yang X-Y, Zhu Y-K, Miura H, Sakai T (2010) Static recrystallization behavior of hot-deformed magnesium alloy AZ31 during isothermal annealing. Trans Nonferr Met Soc China 20:1269–1274

    Article  Google Scholar 

  9. Bacroix B, Driver JH, Le Gall R, Maurice C, Penelle R, Réglé H et al (2004) Dynamic recrystallization and grain growth in a ZK60 magnesium alloy sheet produced by isothermal rolling. Mater Sci Forum 467–470:1175–1180

    Google Scholar 

  10. Eddahbi M, Valle JAd, Pérez-Prado MT, Ruano OA (2005) Comparison of the microstructure and thermal stability of an AZ31 alloy processed by ECAP and large strain hot rolling. Mater Sci Eng, A 410–411:308–311

    Article  Google Scholar 

  11. Kang S-G, Kobayashi T (2004) Grain refinement on AZ31 magnesium alloy by highly strained and annealed method. Mater Sci Forum 449–452:669–672

    Google Scholar 

  12. Huang X, Suzuki K, Chino Y, Mabuchi M (2011) Improvement of stretch formability of Mg–3Al–1Zn alloy sheet by high temperature rolling at finishing pass. J Alloy Compd 509:7579–7584

    Article  Google Scholar 

  13. Huang X, Suzuki K, Saito N (2009) Microstructure and mechanical properties of AZ80 magnesium alloy sheet processed by differential speed rolling. Mater Sci Eng, A 508:226–233

    Article  Google Scholar 

  14. Xia X, Zhang K, Li X, Ma M, Li Y (2013) Microstructure and texture of coarse-grained Mg–Gd–Y–Nd–Zr alloy after hot compression. Mater Des 44:521–527

    Article  Google Scholar 

  15. Peng T, Wang Q, Lin J, Liu M, Roven HJ (2011) Microstructure and enhanced mechanical properties of an Mg–10Gd–2Y–0.5Zr alloy processed by cyclic extrusion and compression. Mater Sci Eng, A 528:1143–1148

    Article  Google Scholar 

  16. Mackenzie LWF, Pekguleryuz M (2008) The influences of alloying additions and processing parameters on the rolling microstructures and textures of magnesium alloys. Mater Sci Eng, A 480:189–197

    Article  Google Scholar 

  17. Abdessameud S, Bradai D (2009) Microstructure and texture evolution in hot rolled and annealed magnesium alloy TRC AZ31. Can Metall Quart 48:433–442

    Article  Google Scholar 

  18. Bale CW, Chartrand P, Degterov SA, Eriksson G, Hack K, Ben Mahfoud R et al (2002) FactSage thermochemical software and databases. CALPHAD 26:189–228

    Article  Google Scholar 

  19. Voorhees PW (1985) The theory of Ostwald ripening. J Stat Phys 38:231–252

    Article  Google Scholar 

  20. Basu I, Al-Samman T (2014) Deformation, recrystallization and grain growth behavior of large-strain hot rolled binary Mg-1Dy alloy, magnesium technology. TMS, Sandiego, pp 133–138

    Google Scholar 

  21. Mackenzie LWF, Pekguleryuz MO (2008) The recrystallization and texture of magnesium–zinc–cerium alloys. Scr Mater 59:665–668

    Article  Google Scholar 

  22. Chino Y, Sassa K, Mabuchi M (2008) Texture and stretch formability of Mg–1.5 mass%Zn–0.2 mass%Ce alloy rolled at different rolling temperatures. Mater Trans 49:2916–2918

    Article  Google Scholar 

Download references

Acknowledgement

The authors would like to thank General Motors, Canada and Natural Sciences and Engineering Research Council of Canada (NSERC) for the financial support.

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Correspondence to Abu Syed Humaun Kabir.

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Kabir, A.S.H., Sanjari, M., Su, J. et al. Effect of annealing on microstructure and texture evolution of uniaxial hot compressed Mg–Al–Sn alloys. J Mater Sci 51, 1600–1609 (2016). https://doi.org/10.1007/s10853-015-9483-1

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  • DOI: https://doi.org/10.1007/s10853-015-9483-1

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