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Multiscale damage characterization in continuous fiber ceramic matrix composites using digital image correlation

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Abstract

Damage in continuous fiber CMCs with weakly bonded fiber–matrix interfaces evolves in several stages that span multiple length scales. Comprehensive damage characterization necessitates identifying how damage initiates as well as how it accumulates (through final failure), which is not feasible with information gathered from a single length scale. Using digital image correlation to measure full-field surface deformations, damage evolutions in continuous fiber SiC/SiC laminates were analyzed at three distinct length scales: constituent, lamina, and laminate. Constituent scale analyses indicated that fine matrix cracks initiated in localized regions of transverse fiber coatings at low stresses. Investigations at the larger lamina scale revealed that some, but not all, of the coating cracks evolved into matrix cracks, the propagation of which was dependent on the state of stress near the crack tip and the local microstructure. Many of these matrix cracks morphed into cracks large enough to be detected at the (largest) laminate scale. The density of the large matrix cracks increased with load, reaching saturation prior to failure. While the constituent scale identifies when (with respect to stress state) and where (with respect to local microstructure) damage initiates, the lamina scale elucidates damage progression between neighboring constituents. Only laminate scale fields of view are large enough to capture the accumulation of the large matrix cracks that ultimately lead to final fracture. However, as spatial resolution is reduced at this scale, finer cracks (which may provide pathways for environmental ingress) go undetected. As each length scale provides a unique perspective of damage evolution in CMCs, multiscale analysis is essential for comprehensive damage characterization.

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References

  1. Zia Z, Curtin W (2008) Multiscale modeling of tensile failure in fiber-reinforced composites. In: Kwon Y, Allen D, Talreja R (eds) Multiscale modeling and simulation of composite materials and structures. Springer, New York, pp 38–82

    Google Scholar 

  2. Ladeveze P, Trovalet M, Lubineau G (2009) A multiscale damage model for the analysis of laminated composite structures on the microscale, 17th International Conference on Composite Materials (ICCM 17), Edinburgh (UK)

  3. Lamon J (2001) A micromechanics-based approach to the mechanical behavior of brittle-matrix composites. J Comput Sci Technol 61:2259–2272

    Article  Google Scholar 

  4. Aveston J, Cooper A, Kelly A (1971) Single and multiple fracture: the properties of fiber composites. IPC Science and Technology Press, pp. 15–26. [Conference Proceedings]

  5. Chawla K (1995) Ceramic matrix composites. Chapman and Hall, London

    Google Scholar 

  6. Aveston J, Kelly A (1973) Theory of multiple fracture of fibrous composites. J Mater Sci 8:52–362. doi:10.1007/BF00550155

    Article  Google Scholar 

  7. Budiansky B, Hutchinson J, Evans A (1986) Matrix fracture in fiber reinforced ceramics. J Mech Phys Solids 34(2):167–189

    Article  Google Scholar 

  8. Solti J, Mall S, Robertson D (1995) Modeling damage in unidirectional ceramic matrix composites. Compos Sci Technol 54:55–66

    Article  Google Scholar 

  9. Beyerle D, Spearing S, Zok F, Evans A (1992) Damage and failure in unidirectional ceramic-matrix composites. J Am Ceram Soc 75(10):19–25

    Article  Google Scholar 

  10. Marshall D, Cox B, Evans A (1985) The mechanics of matrix cracking in brittle matrix fiber composites. Acta Metall 33(11):2013–2021

    Article  Google Scholar 

  11. Curtin W (1993) The tough to brittle transition in brittle matrix composites. J Mech Phys Solids 41:217–245

    Article  Google Scholar 

  12. Spearing S, Zok F, Evans A (1994) Stress corrosion cracking in a unidirectional ceramic matrix composite. J Am Ceram Soc 77(2):562–570

    Article  Google Scholar 

  13. Hutchinson J, Jensen H (1990) Models of fiber debonding and pullout in brittle composites with friction. Mech Mater 9:139–163

    Article  Google Scholar 

  14. Gupta V, Yuan J, Martinez D (1993) Calculation, measurement, and control of interface strength in composites. J Am Ceram Soc 76(2):305–315

    Article  Google Scholar 

  15. Walter ME, Ravichandran G, Oritz M (1997) Computational modeling of damage evolution in unidirectional fiber reinforced ceramic matrix composites. Comput Mech 20:192–198

    Article  Google Scholar 

  16. Evans A (1990) Perspective on the Development of high toughness ceramics. J Am Ceram Soc 73(2):187–206

    Article  Google Scholar 

  17. Evans A, Marshall D (1989) The mechanical behavior of ceramic matrix composites. Acta Metall 37(10):2567–2583

    Article  Google Scholar 

  18. Cox B (1990) Interfacial sliding near a free surface in a fibrous or layered composite during thermal cycling. Acta Metall Mater 38(12):2411–2424

    Article  Google Scholar 

  19. Thouless M, Evans A (1988) Effects of pull-out on the mechanical properties of ceramic-matrix composites. Acta Metall 36(3):517–522

    Article  Google Scholar 

  20. Thouless M, Sbaizero O, Sigl L, Evans A (1989) Effect of interface mechanical properties on pullout in a SiC-fiber-reinforced lithium aluminum silicate glass-ceramic. J Am Ceram Soc 72(4):525–532

    Article  Google Scholar 

  21. Kerans J, Parthasarathy T (1991) Theoretical analysis of the fiber pullout and pushout tests. J Am Ceram Soc 74(7):1585–1596

    Article  Google Scholar 

  22. Sorenson B, Evans R (1993) Analysis of damage in a ceramic matrix composite. Int J Damage Mech 2:246–271

    Article  Google Scholar 

  23. Walter M, Ravichandran G (1995) An experimental investigation of damage evolution in a ceramic matrix composite. J Eng Mater Technol 117:101–108

    Article  Google Scholar 

  24. Daniel J, Anastassopoulos G (1995) Failure mechanisms and damage evolution in crossply ceramic matrix composites. Int J Solids Struct 32(3):341–355

    Article  Google Scholar 

  25. Morscher G (1999) Modal acoustic emission of damage accumulation in a woven SiC/SiC composite. Compos Sci Technol 59:687–697

    Article  Google Scholar 

  26. Rohmer E, Martin E, Lorrette C (2014) Mechanical properties of SiC/SiC braided tubes for fuel cladding. J. Nucl Mater 453:16–21

    Article  Google Scholar 

  27. Bernachy-Barbe F, Gelebart L, Bornert M, Crepin J, Sauder C (2014) Characterization of SiC/SiC composites damage mechanisms using digital image correlation at the tow scale. Compos A 68:101–109

    Article  Google Scholar 

  28. Rossol MN, Shaw JH, Bale H, Ritchie RO, Marshall DB, Zok F (2013) Characterizing weave geometry in textile ceramic composites using digital image correlation. J Am Ceram Soc 96(8):2362–2365

    Article  Google Scholar 

  29. Rajan VP, Rossol MN, Zok FW (2012) Optimization of digital image correlation for high-resolution strain mapping of ceramic composites. Exp Mech 52(9):1407–1421

    Article  Google Scholar 

  30. Kammers AD, Daly S (2011) Small-scale patterning methods for digital image correlation under scanning electron microscopy. Meas Sci Technol 22:125501

    Article  Google Scholar 

  31. Kammers AD, Daly S (2013) Self-assembled nanoparticle surface patterning for improved digital image correlation in a scanning electron microscope. Exp Mech 53:1333–1341

    Article  Google Scholar 

  32. Scrivens WA, Luo Y, Sutton MA, Collete SA, Myrick ML, Miney P, Colavira PE, Reynolds AP, Li X (2007) Development of patterns for digital image correlation measurements at reduced length scales. Exp Mech 47:63–77

    Article  Google Scholar 

  33. Collete SA, Sutton MA, Miney P, Reynolds AP, Li X, Colavita PE, Scrivens WA, Luo Y, Sudarshan T, Muzykov P, Myrick ML (2004) Development of patterns for nanoscale strain measurements: I. fabrication of imprinted Au webs for polymeric materials. Nanotechnology 15:1812–1817

    Article  Google Scholar 

  34. Tracy J, Waas A, Daly S (2015) A new experimental approach for in situ damage assessment in fibrous ceramic matrix composites at high temperature. J Am Ceram Soc. doi:10.1111/jace.13538

    Google Scholar 

  35. Wachtman J, Cannon W, Matthewson M (2009) Mechanical properties of ceramics. Wiley, New York, p 268

    Book  Google Scholar 

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Tracy, J., Daly, S. & Sevener, K. Multiscale damage characterization in continuous fiber ceramic matrix composites using digital image correlation. J Mater Sci 50, 5286–5299 (2015). https://doi.org/10.1007/s10853-015-9076-z

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  • DOI: https://doi.org/10.1007/s10853-015-9076-z

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