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In situ synchrotron X-ray radiation analysis of hydrogen behavior in stainless steel subjected to continuous heating

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Abstract

Hydrogen generally causes lattice distortions and phase transformations when introduced into a metallic crystal lattice. For the investigations reported in this contribution, hydrogen thermal desorption analysis has been carried out to observe the influence of hydrogen desorption on the lattice of super martensitic stainless steel during continuous heating. The lattice expansion parameter and the phase transformations have been monitored during the thermal desorption process, and the influence of hydrogen on such characteristics has been evaluated. It was found that hydrogen has a significant influence on both the lattice parameter and on the thermal expansion. However, hydrogen has no influence on phase transformation during thermal desorption. The hydrogen’s desorption behavior in this process was also observed and it turned out that hydrogen desorbs in two stages, i.e., firstly diffusible hydrogen and trapped hydrogen afterward.

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Acknowledgements

We sincerely thank BESSY II in Berlin Adlershof for allowing the measurement time and providing the required equipment. We also thank Prof. Christoph Genzel and his colleague Manuela Klaus for giving us the appropriate technical support that allowed us to conduct our experiments.

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Authors and Affiliations

  1. BAM Federal Institute for Materials Research and Testing, Unter den Eichen 87, 12205, Berlin, Germany

    E. Dabah, Th. Kannengiesser & Th. Boellinghaus

  2. Department of Materials Engineering, Ben-Gurion University of the Negev, Beer Sheva, Israel

    D. Eliezer

Authors
  1. E. Dabah
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  2. Th. Kannengiesser
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  3. D. Eliezer
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  4. Th. Boellinghaus
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Correspondence to E. Dabah.

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Dabah, E., Kannengiesser, T., Eliezer, D. et al. In situ synchrotron X-ray radiation analysis of hydrogen behavior in stainless steel subjected to continuous heating. J Mater Sci 47, 5879–5885 (2012). https://doi.org/10.1007/s10853-012-6489-9

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  • DOI: https://doi.org/10.1007/s10853-012-6489-9

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