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Effect of annealing on precipitation, microstructural stability, and mechanical properties of cryorolled Al 6063 alloy

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Abstract

The effect of annealing on precipitation, microstructural stability, and mechanical properties of cryorolled Al 6063 alloy has been investigated in the present work employing hardness measurements, tensile test, XRD, DSC, EBSD, and TEM. The solution-treated bulk Al 6063 alloy was subjected to cryorolling to produce ultrafine grain structures and subsequently annealing treatment to investigate its thermal stability. The CR Al 6063 alloys with ultrafine-grained microstructure are thermally stable up to 250 °C as observed in the present work. Within the range of 150–225 °C, the size of small precipitate particles is <1 μm. These small precipitate particles pin the grain boundaries due to Zener drag effect, due to which the grain growth is retarded. The hardness and tensile strength of the cryorolled Al 6063 alloys have decreased upon subjecting it to annealing treatment (150–250 °C).

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References

  1. Burger GB, Gupta AK, Jeffrey PW, Lloyd DJ (1995) Mater Charact 35:23

    Article  CAS  Google Scholar 

  2. Usta M, Glicksman ME, Wright RN (2004) Metall Mater Trans A 35A:435

    Article  CAS  ADS  Google Scholar 

  3. Andersen SJ (1995) Metall Mater Trans A 26A:1931

    Article  CAS  ADS  Google Scholar 

  4. Miller WS, Zhuang L, Bottema J, Wittebrood AJ, Smet PD, Haszler A (2000) Mater Sci Eng A 280:37

    Article  Google Scholar 

  5. A statistical review on Aluminium Shipments by Major Market, United states and Canada, 2004

  6. Wang Y, Chen M, Zhou F, Ma E (2002) Nature 419:912

    Article  CAS  PubMed  ADS  Google Scholar 

  7. Valiev RZ, Islamgaliev RK, Alexandrov IV (2000) Prog Mater Sci 45:103

    Article  CAS  Google Scholar 

  8. Panigrahi SK, Jayaganthan R, Pancholi V (2009) Mater Des 30:1894

    CAS  Google Scholar 

  9. Panigrahi SK, Jayaganthan R, Chawla V (2008) Mater Lett 62:2626

    Article  CAS  Google Scholar 

  10. Panigrahi SK, Jayaganthan R (2008) Mater Sci Forum 584:734

    Article  Google Scholar 

  11. Kim YG, Ko YG, Shin DH, Lee S (2010) Acta Mater 54:2545

    Article  Google Scholar 

  12. Kwan C, Wang Z, Kang SB (2008) Mater Sci Eng A 480:148

    Article  Google Scholar 

  13. Tsuji N, Ito Y, Saito Y, Minamino Y (2002) Scripta Mater 47:893

    Article  CAS  Google Scholar 

  14. Kamikawa N, Tsuji N, Huang X, Hansen N (2006) Acta Mater 54:3055

    Article  CAS  Google Scholar 

  15. Panigrahi SK, Jayaganthan R (2008) Mater Sci Eng A 480:299

    Article  Google Scholar 

  16. Mishra RS, Mukherjee AK (1997) Mater Sci Eng A 234:1023

    Article  Google Scholar 

  17. Ma Y, Furukawa M, Horita Z, Nemoto M, Valiev RZ, Langdon TG (1996) Mater Trans 37:336

    CAS  Google Scholar 

  18. Szczygiel P, Roven HJ, Reiso O (2008) Mater Sci Eng A 493:202

    Article  Google Scholar 

  19. Lee YB, Shin DH, Park KT, Nam WJ (2004) Scripta Mater 51:355

    Article  CAS  Google Scholar 

  20. Cao WQ, Godfrey A, Liu W, Liu Q (2004) Mater Lett 51:3667

    Google Scholar 

  21. Doherty RD, Hughes DA, Humphreys FJ, Jonas JJ, Jensen DJ, Kassner ME, King WE, McNelley TR, McQueen HJ, Rollett AD (1997) Mater Sci Eng A 234–236:219

    Google Scholar 

  22. Rangaraju N, Raghuram T, Krishna BV, Rao KP, Venugopal P (2005) Mater Sci Eng A 398:246

    Article  Google Scholar 

  23. Miao WF, Laughlin DE (1999) Scripta Mater 40:873

    Article  CAS  Google Scholar 

  24. Esmaeili S, Wang SX, Lloyd DJ, Poole WJ (2003) Metall Mater Trans A 34A:751

    CAS  ADS  Google Scholar 

  25. Edwards GA, Stiller K, Dunlop GL, Couper MJ (1998) Acta Mater 46:3893

    Article  CAS  Google Scholar 

  26. Jacobs MH (1972) Philos Mag 26:1

    Article  CAS  ADS  Google Scholar 

  27. Yassar RS, Cai M, Field DP, Chen X, Asay J (2006) J Mater Sci 41:1711. doi:10.1007/s10853-006-0870-5

    Article  CAS  ADS  Google Scholar 

  28. Yassar RS, Field DP, Weiland H (2005) Metall Mater Trans A 36A:2059

    Article  CAS  ADS  Google Scholar 

  29. Buha J, Lumley RN, Crosky AG, Hono K (2007) Acta Mater 55:3015

    Article  CAS  Google Scholar 

  30. Urrutia IG, Munoz-Morris MA, Morris DG (2005) Mater Sci Eng A 394:399

    Article  Google Scholar 

  31. Humphrey FJ, Prangnell PB, Bowen JR, Gholinia A, Harris C (1999) Philos Trans Roy Soc Lond 357A:1663

    Article  ADS  Google Scholar 

  32. Morris DG, Munoz-Morris MA (2002) Acta Mater 50:4047

    Article  CAS  Google Scholar 

  33. Weatherly GC, Perovic A, Mukhopadhyay NK, Llyod DJ, Perovic DD (2001) Metall Mater Trans A 32:213

    Article  Google Scholar 

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Acknowledgements

One of the authors, Dr. Sushanta Kumar Panigrahi, would like to thank CSIR, New Delhi for having supported this work through RA fellowship. Dr. R. Jayaganthan expresses his sincere thanks to DST, New Delhi for their financial grant to this work through Grant no DST-462-MMD.

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Correspondence to R. Jayaganthan.

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Panigrahi, S.K., Jayaganthan, R. Effect of annealing on precipitation, microstructural stability, and mechanical properties of cryorolled Al 6063 alloy. J Mater Sci 45, 5624–5636 (2010). https://doi.org/10.1007/s10853-010-4627-9

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  • DOI: https://doi.org/10.1007/s10853-010-4627-9

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