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Influence of annealing on rheological and conductive behaviors of high-density polyethylene/carbon black composites

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Abstract

A simultaneous measurement on dynamic viscoelastic and conductive behaviors was carried out to investigate the effect of high temperature annealing on the properties of carbon black (CB) filled high-density polyethylene composites. The results showed that dynamic storage and loss moduli of the composites increased significantly with increasing annealing time, and there existed a liquid- to solid-like transition at a critical time (tc) which is dependent on temperature and CB content. Accompanying with the variation in dynamic moduli, electrical resistance (R) decreased sharply with time. What’s more, the increase of R could be observed in the long time region. The activation energy determined from tc as a function of reciprocal temperature was found to be irrespective of CB content. The evolutions of moduli and R induced by thermal treatment were discussed on the base of the concept of filler flocculation in the melt.

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Acknowledgement

This work was supported by the National Nature Science Foundation of China (No. 20774085).

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Authors and Affiliations

  1. Department of Polymer Science and Engineering, Zhejiang University, Hangzhou, 310027, China

    Qing Cao, Yihu Song, Zhihua Liu & Qiang Zheng

  2. Key Laboratory of Macromolecular Synthesis and Functionalization of Ministry of Education, Zhejiang University, Hangzhou, 310027, China

    Qing Cao, Yihu Song, Zhihua Liu & Qiang Zheng

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  1. Qing Cao
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  2. Yihu Song
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  3. Zhihua Liu
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  4. Qiang Zheng
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Correspondence to Qiang Zheng.

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Cao, Q., Song, Y., Liu, Z. et al. Influence of annealing on rheological and conductive behaviors of high-density polyethylene/carbon black composites. J Mater Sci 44, 4241–4245 (2009). https://doi.org/10.1007/s10853-009-3590-9

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  • DOI: https://doi.org/10.1007/s10853-009-3590-9

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