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Hydroxyapatite deposition study through polymeric process on commercially pure Ti surfaces modified by laser beam irradiation

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Abstract

Many techniques have been used to coat metallic substrate with bioceramics. The aim of this study was to study the physical-chemical characteristics of polyvinylidene fluoride (α-PVDF)/hydroxyapatite (HA) composite coating, obtained by casting method, on commercially pure titanium (α-CP Ti) substrate surface modified by laser beam irradiation. The preparation of coating was done for mixing α-PVDF pellets shape dissolved in dimethylacetamide (DMA) with HA/DMA emulsion. The mixture was poured onto the α-CP Ti sample and left to dry in an oven. CP Ti plates were coated with α-PVDF/HA composite film, in proportions of 100/00 and 60/40 in weight, and characterized by particle size analysis, scanning electron microscopy, energy dispersive spectroscopy (EDS), X-ray diffractometry, thickness measurement and contact angle. Uniform coating with a small thickness variation along the coated surface was successfully obtained.

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References

  1. Tajima K, Hironaka M, Chen K, Nagamatsu Y, Kakigawa H, Kozono Y (2008) Dent Mater J 27:258

    Article  PubMed  CAS  Google Scholar 

  2. Suchanek W, Yoshimura M (1998) J Mater Res 13:94. doi:10.1557/JMR.1998.0015

    Article  ADS  CAS  Google Scholar 

  3. Kweh SWK, Khor KA, Cheang P (2000) Biomaterials 21:1223

    Article  PubMed  CAS  Google Scholar 

  4. Arias JL, Mayor MB, Pou J, Leng Y, León B, Pérez-Amor M (2003) Biomaterials 24:3403. doi:10.1016/S0142-9612(03)00202-3

    Article  PubMed  CAS  Google Scholar 

  5. Metikos-Hukovic M, Tkalcec E, Kwokal A, Piljac J (2003) Surf Coat Technol 165:40

    Article  CAS  Google Scholar 

  6. Abe Y, Kokubo T, Yamamuro T (1990) J Mater Sci: Mater Med 1:233. doi:10.1007/BF00701082

    Article  CAS  Google Scholar 

  7. Brendel T, Engel A, Rüssel C (1992) J Mater Sci: Mater Med 3:175. doi:10.1007/BF00713445

    Article  CAS  Google Scholar 

  8. Lacefield WR (1993) In: Hench LL, Wilson J (eds) Advanced series in ceramics. World Scientific Publishing, Singapore

    Google Scholar 

  9. Fatehi K, Moztarzadeh F, Solati-hashjin M, Tahriri M, Rezvannia M, Ravarian R (2008) Bull Mater Sci 31:101

    Article  CAS  Google Scholar 

  10. Inderherbergh J (1991) Ferroelectrics 115:295. doi:10.1080/00150199108222386

    CAS  Google Scholar 

  11. Callegari B, Belangero WD (2004) Acta Ortop Bras 12:160

    Article  Google Scholar 

  12. Campos JSC, Ribeiro AA, Cardoso CX (2007) Mater Sci Eng B 136:123. doi:10.1016/j.mseb.2006.09.017

    Article  CAS  Google Scholar 

  13. Braga FJC, Marques RFC, Filho EA, Guastaldi AC (2007) App Surf Sci 253:9203. doi:10.1016/j.apsusc.2007.05.048

    Article  ADS  CAS  Google Scholar 

  14. Braga FJC, Rogero SO, Couto AA, Marques RFC, Ribeiro AA, Campos JSC (2007) Mater Res 10:247. doi:10.1590/S1516-14392007000300005

    CAS  Google Scholar 

  15. Ribeiro AA (2007) Doctoral thesis, State University of Campinas, Campinas, Brazil

  16. Cam-micro (1996) Contact angle meter model Cam-micro, operating manual. Tantec Inc., Schaumburg, IL

    Google Scholar 

  17. Adam NK (1963) In: Moilliet JL (ed) Waterproofing and water-repellency. Elsevier, Amsterdam

    Google Scholar 

  18. Sheldon RP (1982) Composite polymeric materials. Applied Science Publishers, London

    Google Scholar 

  19. Park JB (1984) Biomaterials science and engineering. Plenum Press, New York

    Google Scholar 

  20. Powder diffraction file (PDF) (2000) International Centre for Diffraction Data-Joint Committee of Powder Diffraction Standards (ICDD-JCPDS)

  21. Lovinger AJ (1982) In: Basset DC (ed) Developments in crystalline polymers—1. Applied Science Publishers Ltd, London

    Google Scholar 

  22. Moita JMN (2006) Brazil FAPEPI, Terezina. www.fapepi.pi.gov.br/novafapepi/ciencia/documentos/Molhamento.PDF. Accessed 4 Dec 2007

Download references

Acknowledgement

The authors thank to the Department of Polymer Technology/School of Chemical Engineering/State University of Campinas, Department of Physical Chemistry/Institute of Chemistry/São Paulo State University and Department of Applied Physics/Gleb Wataghin Physics Institute/State University of Campinas, for their technical support, and CAPES (Brazil) for granting a fellowship.

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Correspondence to Alexandre Antunes Ribeiro.

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Ribeiro, A.A., Marques, R.F.C., Guastaldi, A.C. et al. Hydroxyapatite deposition study through polymeric process on commercially pure Ti surfaces modified by laser beam irradiation. J Mater Sci 44, 4056–4061 (2009). https://doi.org/10.1007/s10853-009-3585-6

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  • DOI: https://doi.org/10.1007/s10853-009-3585-6

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