Abstract
In order to study model microstructures representative of industrial refractory materials, this work is devoted to the elaboration and microstructural characterisation of two-phase model materials able to develop interfacial damage by thermal expansion mismatch between the matrix and inclusions. The studied materials are composed of a vitreous matrix surrounding dense alumina balls (Al2O3 99.9%). As expected, because of the not null dilatometric dissension (Δα < 0 with αmatrix < αinclusions), all the samples exhibit partial decohesions at the matrix-inclusions interfaces. But one also observes the presence of two types of unexpected cracks: straight cracks in the median plane between two inclusions and circular cracks around inclusions. Numerical, analytical and experimental tools were used to study the origin of such unexpected defects.
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Acknowledgements
Yoann Joliff would like to express his gratitude towards the Limousin Region and the European Social Fund for financial support of the present work.
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Joliff, Y., Absi, J., Huger, M. et al. Microcracks with unexpected characteristics induced by CTE mismatch in two-phase model materials. J Mater Sci 43, 330–337 (2008). https://doi.org/10.1007/s10853-007-1691-x
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DOI: https://doi.org/10.1007/s10853-007-1691-x