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Influence of the synthesis methods on the particle size of the LiVMoO6 phase

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Abstract

The lithiated transition metal oxide LiVMoO6 has been synthesized by a novel melt quenching method that presents some advantages as compared to the classical solid-state reaction and soft-combustion synthesis. These are: the short preparation time and the possibility to control the grain size of LiVMoO6 powders. The local structure of LiVMoO6 samples prepared in different ways was characterized by IR spectral analysis. The oxidation state of Li, V, and Mo was determined by X-ray photoelectron spectroscopy.

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Authors and Affiliations

  1. Institute of General and Inorganic Chemistry, Bulgarian Academy of Sciences, 1113, Sofia, Bulgaria

    Margarita Milanova, Reni Iordanova & Krassimir Kostov

  2. University of Chemical Technology and Metallurgy, Sofia, 1756, Bulgaria

    Yanko Dimitriev

  3. Institute of Electrochemistry and Energy Systems, 1113, Sofia, Bulgaria

    Sasho Vassilev

Authors
  1. Margarita Milanova
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  2. Reni Iordanova
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  3. Yanko Dimitriev
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  4. Krassimir Kostov
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  5. Sasho Vassilev
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Correspondence to Margarita Milanova.

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Milanova, M., Iordanova, R., Dimitriev, Y. et al. Influence of the synthesis methods on the particle size of the LiVMoO6 phase. J Mater Sci 42, 3349–3352 (2007). https://doi.org/10.1007/s10853-006-1169-2

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  • DOI: https://doi.org/10.1007/s10853-006-1169-2

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