Abstract
Fluorescence microprobe spectroscopy was used to characterize the stress fields that develop within an interpenetrating Al–Al2O3 composite resulting from both the thermal expansion mismatch during sample processing, and from an external applied load. The 30 vol% Al–70 vol% Al2O3 composite that was investigated had an aluminum and alumina phase feature size of 50–100 μm. The residual thermal compressive stress measured in the alumina was ∼40–340 MPa. The effect of varying the metal ligament size on the residual stress distribution is discussed. Additionally, the application of an external load caused a non-uniform stress distribution to develop within the alumina regions around the crack-tip, which was attributed to microstructure inhomogeneities. The crack was further extended and the influence of the stress distribution within the alumina regions on the crack extension direction is briefly discussed.
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References
Venkateswara Rao KT, Soboyelo WO, Ritchie RO (1992) Metall Trans A 23A:2249
Badrinarayanan K, McKelvey AL, Venkateswara Rao KT, Ritchie RO (1996) Metall Trans A 27A:3781
Bloyer DR, Venkateswara Rao KT, Ritchie RO (1998) Metall Trans A 29A:2483
Prielipp H, Knechtel M, Claussen N, Streiffer S, Müllejans H, Rühle M, Rödel J (1995) Mater Sci Engng 197A:19
Neubrand A, Chung T-J, Rödel J, Steffler ED, Fett T (2002) J Mater Res 17(11):2912
Moon RJ, Tilbrook M, Hoffman M, Neubrand A (2005) J Am Ceramic Soc 88(3):666
Hoffman M, Skirl S, Pompe W, Rödel J (1999) Acta Mater 47:565
Hoffman M, Fiedler B, Emmel T, Prielipp H, Claussen N, Gross D, Rödel J (1997) Acta mater 45:3609
Skirl S, Hoffman M, Bowman K, Wiederhorn S, Rödel J (1998) Acta Mater 46:2493
Hoffman M, Rödel J, Skirl S, Zimmermann A, Fuller E, Mullejans H (1999) Key Eng Mater 159–160:311
Ashby MF, Blunt FJ, Bannister M (1989) Acta Metall 37:1847
Pezzotti G, Muller WH (2002) Continuum Mech Thermodyn 14:113
Wang C, Libardi W, Baldo JB (1998) Int J Fracture 94:177
Kassam ZHA, Zhang RJ, Wang Z (1995) Mat Sci Eng A203:286
Li Z, Chen Q (2003) Eng Frac Mech 70:581
Butcher RJ, Rousseau CE, Tippur HV (1999) Acta Mater 47(1):259
Kubler J (1997) Ceram Eng Sci Proc 18:155
Pezzotti G, Sbaizero O (2001) Mat Sci Eng A303:267
He J, Clarke DR (1995) J Am Ceram Soc 78:1347
Ma Q, Clarke DR (1993) J Am Ceram Soc 76:1433
Tilbrook M, Moon R, Hoffman M (2005) Mat Sci Eng A393:170
ASTM Standard E 1820-96 (1997) Standard test method for measurement of fracture toughness. ASTM, Philadelphia, Pa
Agrawal P, Conlon K, Bowman KJ, Sun CT, Chichocki FR Jr, Trumble KP (2003) Acta Mater 51:1143
Acknowledgements
The authors sincerely thank Prof. Jürgen Rödel of the Technische Universitaet Darmstadt, Germany for use of equipment and assistance during sample preparation. Additionally, the authors would like to thank Lyndal Rutgers of the University of New South Wales for providing the epoxy-alumina sample. This work was supported by the Australian Research Council, the Australian Academy of Science and the Japan Society for the Promotion of Science.
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Moon, R.J., Hoffman, M., Tochino, S. et al. Fluorescence spectroscopy analysis of Al–Al2O3 composites with coarse interpenetrating networks. J Mater Sci 41, 7571–7579 (2006). https://doi.org/10.1007/s10853-006-0843-8
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DOI: https://doi.org/10.1007/s10853-006-0843-8