Abstract
Weibull modulus of bending strength of nanolayer-grained ceramic Ti3SiC2 was estimated with over 50 specimens, using the least square method, the moment method and the maximum likelihood technique, respectively. The result demonstrated that the m-value of this layered ceramic ranged from 25 to 29, which is much higher than that of traditional brittle ceramics. The reason of high Weibull modulus was due to high damage tolerance of this material. Under stress, delamination and kinking of grains and shear slipping at interfaces give this material high capacity of local energy dissipation and easy local stress relaxation, leading to the excellent damage tolerance of Ti3SiC2. The effect of amounts of specimens on the reliability of the estimated m-values was also investigated. It was confirmed that the stability of the estimated m-value increased with increasing numbers of specimens. The parameter obtained using the maximum likelihood technique showed the highest reliability than other methods. The ranges of failure probability were determined using the Weibull estimates calculated from the maximum likelihood technique.
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References
Davidge RW (1979) Mechanical behavior of ceramics. Cambridge University Press, UK
Papargyris AD (1998) J Eur Ceram Soc 18:451
Weibull W (1951) J Appl Mech 18:253
Bergman W (1987) In: Freer R, Newsam S, Syers G (eds) Engineering with ceramics 2. British Ceramic Proceeding No. 39, Dec. 1987, p 175
Gong JH, Li Y (1999) J Am Ceram Soc 82:449
ISO/TC 206/FDIS 20501:2003(E), Fine ceramics – Weibull statistics of strength data, 2003
Bao YW, Wang W, Zhou YC (2004) Acta Mater 52:5397
Bao YW, Hu CF, Zhou YC (2006) Mater Sci Technol 21:27
Kooi BJ, Poppen RJ, Carvalho NJM, Hosson JThM, Barsoum MW (2003) Acta Mater 51:2859
Bao YW, Chen JX, Wang XH, Zhou YC (2004) J Eur Ceram Soc 24:855
Tzenov NV, Barsoum MW (2000) J Am Ceram Soc 83:825
Barsoun MW, El-Raghy T (1996) J Am Ceram Soc 79:1953
Wang XH, Zhou YC (2002) Acta Mater 50:3141
Low IM, Lee SK, Lawn BR, Barsoum MW (1998) J Am Ceram 81:225
Dcosta DJ, Sun W, Lin F, El-Raghy T (2002) J Mater Process Tech 127:352
El-Raghy T, Zavaliangos A, Barsoum MW, Kalidindi SR (1997) J Am Ceram Soc 80:513
Acknowledgements
This work was supported by the National Outstanding Young Scientist Foundation (No. 50125204 for Y. Bao and No.59925208 for Y. Zhou), National Science Foundation of China under Grant No. 50672093, 50302011, 90403027 and “The Hundred-talent plan” of Chinese Academy of Sciences and “863” program.
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Bao, Y.W., Zhou, Y.C. & Zhang, H.B. Investigation on reliability of nanolayer-grained Ti3SiC2 via Weibull statistics. J Mater Sci 42, 4470–4475 (2007). https://doi.org/10.1007/s10853-006-0427-7
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DOI: https://doi.org/10.1007/s10853-006-0427-7